(-)-(1'S)-8-benzyloxy-3-(1'-hydroxyethyl)-5-methoxy-1,2-dihydronaphthalene

Base Information

Chemical Name:(-)-(1'S)-8-benzyloxy-3-(1'-hydroxyethyl)-5-methoxy-1,2-dihydronaphthalene
CAS No.:96236-40-7
Molecular Formula:C₂₀H₂₂O₃
Molecular Weight:310.393
Hs Code.:

Synonyms:(-)-(1'S)-8-benzyloxy-3-(1'-hydroxyethyl)-5-methoxy-1,2-dihydronaphthalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(1'S)-8-benzyloxy-3-(1'-hydroxyethyl)-5-methoxy-1,2-dihydronaphthalene

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Technology Process of (-)-(1'S)-8-benzyloxy-3-(1'-hydroxyethyl)-5-methoxy-1,2-dihydronaphthalene

There total 1 articles about (-)-(1'S)-8-benzyloxy-3-(1'-hydroxyethyl)-5-methoxy-1,2-dihydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 89144-50-3
3-acetyl-8-benzyloxy-5-methoxy-1,2-dihydronaphthalene

: 96236-40-7
(-)-(1'S)-8-benzyloxy-3-(1'-hydroxyethyl)-5-methoxy-1,2-dihydronaphthalene

Guidance literature:: With lithium aluminium tetrahydride; (-)-N-methylephedrine; N-ethyl-N-phenylamine; In diethyl ether; at -78 ℃; for 1h;
DOI:10.1071/CH9850179

Reference yield:

: 96236-40-7
(-)-(1'S)-8-benzyloxy-3-(1'-hydroxyethyl)-5-methoxy-1,2-dihydronaphthalene

: (S)-1-(4-Benzyloxy-7-methoxy-3,7b-dihydro-2H-1-oxa-cyclopropa[a]naphthalen-1a-yl)-ethanol

Guidance literature:: With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; In benzene; for 1.5h;
DOI:10.1071/CH9850179

Reference yield:

: 96236-40-7
(-)-(1'S)-8-benzyloxy-3-(1'-hydroxyethyl)-5-methoxy-1,2-dihydronaphthalene

: 90744-26-6
(-)-(2R,1'S)-5-benzyloxy-2-(1'-hydroxyethyl)-8-methoxy-1,2,3,4-tetrahydronaphthalen-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: vanadium(IV) bis(pentane-2,4-dionate) oxide, t-butyl hydroperoxide / benzene / 1.5 h

2: 77 percent / LiAlH₄ / benzene; diethyl ether / Ambient temperature

With tert.-butylhydroperoxide; lithium aluminium tetrahydride; bis(acetylacetonate)oxovanadium; In diethyl ether; benzene;
DOI:10.1071/CH9850179