[(dibenzyloxyphosphorylmethyl)benzyloxyphosphinoylmethyl]phosphonic acid methyl ester

Base Information

• Chemical Name: [(dibenzyloxyphosphorylmethyl)benzyloxyphosphinoylmethyl]phosphonic acid methyl ester
• CAS No.: 1010804-51-9
• Molecular Formula: C₂₄H₂₉O₈P₃
• Molecular Weight: 538.411

Synonyms:[(dibenzyloxyphosphorylmethyl)benzyloxyphosphinoylmethyl]phosphonic acid methyl ester

Chemical Property of [(dibenzyloxyphosphorylmethyl)benzyloxyphosphinoylmethyl]phosphonic acid methyl ester

Chemical Property:

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Technology Process of [(dibenzyloxyphosphorylmethyl)benzyloxyphosphinoylmethyl]phosphonic acid methyl ester

There total 1 articles about [(dibenzyloxyphosphorylmethyl)benzyloxyphosphinoylmethyl]phosphonic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

[(dibenzyloxyphosphorylmethyl)benzyloxyphosphinoylmethyl]phosphonic acid dimethyl ester (1010804-50-8) → [(dibenzyloxyphosphorylmethyl)benzyloxyphosphinoylmethyl]phosphonic acid methyl ester (1010804-51-9)

Guidance literature:

[(dibenzyloxyphosphorylmethyl)benzyloxyphosphinoylmethyl]phosphonic acid dimethyl ester; With potassium cyanide; In N,N-dimethyl-formamide; at 75 ℃; for 5h;

With Dowex-H(+); In methanol; water; for 4h; Further stages.;

DOI:10.1021/jo702249j

Reference yield: 72.0%

[(dibenzyloxyphosphorylmethyl)benzyloxyphosphinoylmethyl]phosphonic acid methyl ester (1010804-51-9) + {1-[3,4-bis(benzoyloxy)-5-hydroxymethyltetrahydrofuran-2-yl]-2-oxo-2,3-dihydro-1H-pyrimidin-4-ylidenemethyl}phosphonic acid dimethyl ester (1010804-46-2) → {1-[3,4-bis(benzoyloxy)-5-(bis[(benzyloxyphosphorylmethyl)benzyloxyphosphorylmethyl]methyloxyphosphoryl)-tetrahydrofuran-2-yl]-2-oxo-2,3-dihydro-1H-pyrimidin-4-ylidenemethyl}phosphonic acid dimethyl ester

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 3.5h;

DOI:10.1021/jo702249j

Reference yield: 68.0%

[(dibenzyloxyphosphorylmethyl)benzyloxyphosphinoylmethyl]phosphonic acid methyl ester (1010804-51-9) + [difluoro{1-[3,4-bis-(acetyloxy)-5-hydroxymethyltetrahydrofuran-2-yl]-2-oxo-1,2-dihydro-pyridin-4-yl}methyl]phosphonic acid diethyl ester (1010804-42-8) → [difluoro{1-[3,4-bis(acetoxy)-5-(bis[(benzyloxyphosphorylmethyl)benzyloxyphosphorylmethyl]methyloxyphosphoryl)-tetrahydrofuran-2-yl]-2-oxo-1,2-dihydro-pyridin-4-yl}methyl]phosphonic acid diethyl ester (1010804-55-3)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 3.5h;

DOI:10.1021/jo702249j

upstream raw materials:

[(dibenzyloxyphosphorylmethyl)benzyloxyphosphinoylmethyl]phosphonic acid dimethyl ester

Downstream raw materials:

[difluoro{1-[3,4-bis(acetoxy)-5-(bis[(benzyloxyphosphorylmethyl)benzyloxyphosphorylmethyl]methyloxyphosphoryl)-tetrahydrofuran-2-yl]-2-oxo-1,2-dihydro-pyridin-4-yl}methyl]phosphonic acid diethyl ester

2',3'-di-O-acetyl-5'-(bis[(benzyloxyphosphorylmethyl)benzyloxyphosphorylmethyl]methyloxyphosphoryl)cytidine 4-N-[O,O-bis(2-cyanoethyl)phosphoramidate]

1-(2',3'-di-O-benzoyl-5'-(bis-[(benzyloxyphosphorylmethyl)benzyloxyphosphorylmethyl]methyloxyphosphoryl)-β-D-ribofuranosyl)-2-oxo-1,2-dihydropyridine

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