{1-[3,4-bis(benzoyloxy)-5-hydroxymethyltetrahydrofuran-2-yl]-2-oxo-2,3-dihydro-1H-pyrimidin-4-ylidenemethyl}phosphonic acid dimethyl ester

Base Information

• Chemical Name: {1-[3,4-bis(benzoyloxy)-5-hydroxymethyltetrahydrofuran-2-yl]-2-oxo-2,3-dihydro-1H-pyrimidin-4-ylidenemethyl}phosphonic acid dimethyl ester
• CAS No.: 1010804-46-2
• Molecular Formula: C₂₆H₂₇N₂O₁₀P
• Molecular Weight: 558.482

Synonyms:{1-[3,4-bis(benzoyloxy)-5-hydroxymethyltetrahydrofuran-2-yl]-2-oxo-2,3-dihydro-1H-pyrimidin-4-ylidenemethyl}phosphonic acid dimethyl ester

Chemical Property of {1-[3,4-bis(benzoyloxy)-5-hydroxymethyltetrahydrofuran-2-yl]-2-oxo-2,3-dihydro-1H-pyrimidin-4-ylidenemethyl}phosphonic acid dimethyl ester

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Technology Process of {1-[3,4-bis(benzoyloxy)-5-hydroxymethyltetrahydrofuran-2-yl]-2-oxo-2,3-dihydro-1H-pyrimidin-4-ylidenemethyl}phosphonic acid dimethyl ester

There total 1 articles about {1-[3,4-bis(benzoyloxy)-5-hydroxymethyltetrahydrofuran-2-yl]-2-oxo-2,3-dihydro-1H-pyrimidin-4-ylidenemethyl}phosphonic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

{1-[3,4-bis(benzoyloxy)-5-(benzoyloxymethyl)tetrahydrofuran-2-yl]-2-oxo-2,3-dihydro-1H-pyrimidin-4-ylidene}methylphosphonic acid dimethyl ester (918299-62-4) → {1-[3,4-bis(benzoyloxy)-5-hydroxymethyltetrahydrofuran-2-yl]-2-oxo-2,3-dihydro-1H-pyrimidin-4-ylidenemethyl}phosphonic acid dimethyl ester (1010804-46-2)

Guidance literature:

With methanol; di(tert-butyl)chlorotinhydroxide dimer; at 66 ℃; for 48h;

DOI:10.1021/jo702249j

Reference yield: 72.0%

[(dibenzyloxyphosphorylmethyl)benzyloxyphosphinoylmethyl]phosphonic acid methyl ester (1010804-51-9) + {1-[3,4-bis(benzoyloxy)-5-hydroxymethyltetrahydrofuran-2-yl]-2-oxo-2,3-dihydro-1H-pyrimidin-4-ylidenemethyl}phosphonic acid dimethyl ester (1010804-46-2) → {1-[3,4-bis(benzoyloxy)-5-(bis[(benzyloxyphosphorylmethyl)benzyloxyphosphorylmethyl]methyloxyphosphoryl)-tetrahydrofuran-2-yl]-2-oxo-2,3-dihydro-1H-pyrimidin-4-ylidenemethyl}phosphonic acid dimethyl ester

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 3.5h;

DOI:10.1021/jo702249j

upstream raw materials:

{1-[3,4-bis(benzoyloxy)-5-(benzoyloxymethyl)tetrahydrofuran-2-yl]-2-oxo-2,3-dihydro-1H-pyrimidin-4-ylidene}methylphosphonic acid dimethyl ester

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