2-Bromo-3,6-dimethylpyridine

Base Information

• Chemical Name: 2-Bromo-3,6-dimethylpyridine
• CAS No.: 38749-92-7
• Molecular Formula: C₇H₈BrN
• Molecular Weight: 186.051
• European Community (EC) Number: 860-456-9
• DSSTox Substance ID: DTXSID101309397

Synonyms:2-bromo-3,6-dimethylpyridine;38749-92-7;SCHEMBL9919116;DTXSID101309397;AKOS024062922;AB65454;CS-0308674;EN300-127051

Chemical Property of 2-Bromo-3,6-dimethylpyridine

Chemical Property:

• Vapor Pressure: 0.142mmHg at 25°C
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 184.98401
• Heavy Atom Count: 9
• Complexity: 94.9

Purity/Quality:

99% ^*data from raw suppliers

2-bromo-3,6-dimethylpyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(N=C(C=C1)C)Br

Technology Process of 2-Bromo-3,6-dimethylpyridine

There total 2 articles about 2-Bromo-3,6-dimethylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

2,5-dimethylpyridine (589-93-5) → 2-bromo-3,6-dimethyl-pyridine (38749-92-7) + 2,5-dimethyl-3-bromopyridine (17117-19-0) + 2,5-Dibromo-3,6-dimethylpyridine (38749-93-8)

Guidance literature:

With sulfuric acid; bromine; at 155 - 175 ℃; for 24h;

Reference yield:

→ 2-bromo-3,6-dimethyl-pyridine (38749-92-7)

Guidance literature:

2.5-Lutidin, Brom;

Reference yield: 80.0%

2-bromo-3,6-dimethyl-pyridine (38749-92-7) + C10H16BFO2Si → C17H22FNSi

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 90 ℃; for 24h; Inert atmosphere;

upstream raw materials:

2,5-dimethylpyridine

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