di-μ-methylimino(methylthio)methanethiolato-bis(tricarbonylmanganese)

Base Information

Chemical Name:di-μ-methylimino(methylthio)methanethiolato-bis(tricarbonylmanganese)
CAS No.:57417-84-2
Molecular Formula:C₁₂H₁₂Mn₂N₂O₆S₄
Molecular Weight:518.377
Hs Code.:

Synonyms:di-μ-methylimino(methylthio)methanethiolato-bis(tricarbonylmanganese)

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Chemical Property of di-μ-methylimino(methylthio)methanethiolato-bis(tricarbonylmanganese)

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Technology Process of di-μ-methylimino(methylthio)methanethiolato-bis(tricarbonylmanganese)

There total 1 articles about di-μ-methylimino(methylthio)methanethiolato-bis(tricarbonylmanganese) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 1.0%

: 14516-54-2
bromopentacarbonylmanganese(I)

: 74-93-1
methylthiol

: 7646-69-7
sodium hydride

: 556-61-6
methyl thioisocyanate

: 10170-69-1
dimanganese decacarbonyl

: 21321-38-0
[(Mn(CO)4(μ-SMe))2]

: 69057-58-5
Mn(CO)4(S₂CN(H)CH₃)

: 55173-11-0
Mn(CO)4(S₂CSCH₃)

: 57417-84-2
di-μ-methylimino(methylthio)methanethiolato-bis(tricarbonylmanganese)

Guidance literature:: In tetrahydrofuran; absence of air and moisture; bubbling MeSH through NaH suspn. (0°C, 2 min), addn. of excess MeNCS, addn. of Mn-complex, warming to room temp. during 2 h; evapn., extn. into CH2Cl2, evapn., chromy. (SiO2, hexane, then CH2Cl2/hexane=1:9, 1:4, 1:2); IR spectroscopy;
DOI:10.1039/DT9780001247