propyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:propyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:83562-57-6
Molecular Formula:C₅₂H₅₉NO₁₂
Molecular Weight:890.04
Hs Code.:

Synonyms:propyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of propyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of propyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 5 articles about propyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72366-33-7
propyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 83562-57-6
propyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / silver triflate, 1,1,3,3-tetramethylurea / CH₂Cl₂

2: 1.) diazabicyclo<2.2.2>octane, (Ph₃P)3RhCl, 2.) HgO, HgCl₂ / 1.) EtOH, reflux, 5 h 2.) Me₂CO, H₂O, 5 min

With 1,4-diaza-bicyclo[2.2.2]octane; Wilkinson's catalyst; silver trifluoromethanesulfonate; tetramethylurea; mercury dichloride; mercury(II) oxide; In dichloromethane;
DOI:10.1021/ja00389a061

Reference yield:

: 83562-55-4
propyl O-(2-O-benzoyl-3,6-di-O-benzyl-4-O-(tetrahydro-2-pyranyl)-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 83562-57-6
propyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With acetic acid; In methanol; water; for 1h; Yield given; Heating;
DOI:10.1021/ja00389a061

Reference yield:

: 78878-50-9
4-O-allyl-2-O-benzoyl-3,6-di-O-benzyl-α-D-galactopyranosyl chloride

: 83562-57-6
propyl O-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / silver triflate, 1,1,3,3-tetramethylurea / CH₂Cl₂

2: 1.) diazabicyclo<2.2.2>octane, (Ph₃P)3RhCl, 2.) HgO, HgCl₂ / 1.) EtOH, reflux, 5 h 2.) Me₂CO, H₂O, 5 min

With 1,4-diaza-bicyclo[2.2.2]octane; Wilkinson's catalyst; silver trifluoromethanesulfonate; tetramethylurea; mercury dichloride; mercury(II) oxide; In dichloromethane;
DOI:10.1021/ja00389a061