propyl O-(4-O-allyl-2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:propyl O-(4-O-allyl-2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:83562-54-3
Molecular Formula:C₅₅H₆₃NO₁₂
Molecular Weight:930.105
Hs Code.:

Synonyms:propyl O-(4-O-allyl-2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of propyl O-(4-O-allyl-2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of propyl O-(4-O-allyl-2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 1 articles about propyl O-(4-O-allyl-2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 72366-33-7
propyl 2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 78878-50-9
4-O-allyl-2-O-benzoyl-3,6-di-O-benzyl-α-D-galactopyranosyl chloride

: 83562-54-3
propyl O-(4-O-allyl-2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; tetramethylurea; In dichloromethane;
DOI:10.1021/ja00389a061

Reference yield: 92.0%

: 83562-54-3
propyl O-(4-O-allyl-2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 83562-56-5
propyl O-(4-O-allyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With sodium; In methanol; for 0.25h; Heating;
DOI:10.1021/ja00389a061

Reference yield:

: 83562-54-3
propyl O-(4-O-allyl-2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-2-acetamido-4,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: N-[(2R,3R,4R,5S,6R)-5-Benzyloxy-4-((2R,3R,4S,5S,6R)-4-benzyloxy-6-benzyloxymethyl-3,5-dihydroxy-tetrahydro-pyran-2-yloxy)-6-benzyloxymethyl-2-propoxy-tetrahydro-pyran-3-yl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) diazabicyclo<2.2.2>octane, (Ph₃P)3RhCl, 2.) HgO, HgCl₂ / 1.) EtOH, reflux, 5 h 2.) Me₂CO, H₂O, 5 min

2: NaOMe / methanol / 0.5 h / Heating

With 1,4-diaza-bicyclo[2.2.2]octane; Wilkinson's catalyst; sodium methylate; mercury dichloride; mercury(II) oxide; In methanol;
DOI:10.1021/ja00389a061