Technology Process of 3,6,7,8,2’,5’-hexamethoxyflavone
There total 4 articles about 3,6,7,8,2’,5’-hexamethoxyflavone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
for 3h;
Reflux;
Inert atmosphere;
DOI:10.1055/s-0035-1561851
- Guidance literature:
-
Multi-step reaction with 4 steps
1: boron trifluoride diethyl etherate / Inert atmosphere
2: potassium hydroxide / ethanol / 73 h / 0 - 20 °C / Inert atmosphere
3: dihydrogen peroxide; sodium hydroxide / water / 24 h / 20 °C / Inert atmosphere
4: potassium carbonate / acetone / 3 h / Reflux; Inert atmosphere
With
boron trifluoride diethyl etherate; dihydrogen peroxide; potassium carbonate; potassium hydroxide; sodium hydroxide;
In
ethanol; water; acetone;
2: |Claisen-Schmidt Condensation / 3: |Algar-Flynn-Olyamada Reaction;
DOI:10.1055/s-0035-1561851
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium hydroxide / ethanol / 73 h / 0 - 20 °C / Inert atmosphere
2: dihydrogen peroxide; sodium hydroxide / water / 24 h / 20 °C / Inert atmosphere
3: potassium carbonate / acetone / 3 h / Reflux; Inert atmosphere
With
dihydrogen peroxide; potassium carbonate; potassium hydroxide; sodium hydroxide;
In
ethanol; water; acetone;
1: |Claisen-Schmidt Condensation / 2: |Algar-Flynn-Olyamada Reaction;
DOI:10.1055/s-0035-1561851
