6-chloro-1-cyclohexylmethyl-3-[2-(diethylamino)ethyl]-2,3-dihydro-4(1H)-quinazolinone

Base Information

Chemical Name:6-chloro-1-cyclohexylmethyl-3-[2-(diethylamino)ethyl]-2,3-dihydro-4(1H)-quinazolinone
CAS No.:159794-16-8
Molecular Formula:C₂₁H₃₂ClN₃O
Molecular Weight:377.958
Hs Code.:

Synonyms:6-chloro-1-cyclohexylmethyl-3-[2-(diethylamino)ethyl]-2,3-dihydro-4(1H)-quinazolinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-chloro-1-cyclohexylmethyl-3-[2-(diethylamino)ethyl]-2,3-dihydro-4(1H)-quinazolinone

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Technology Process of 6-chloro-1-cyclohexylmethyl-3-[2-(diethylamino)ethyl]-2,3-dihydro-4(1H)-quinazolinone

There total 5 articles about 6-chloro-1-cyclohexylmethyl-3-[2-(diethylamino)ethyl]-2,3-dihydro-4(1H)-quinazolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2550-36-9
Cyclohexylmethyl bromide

: 159793-94-9
6-chloro-3-[2-(diethylamino)ethyl]-2,3-dihydro-4(1H)-quinazolinone

: 159794-16-8
6-chloro-1-cyclohexylmethyl-3-[2-(diethylamino)ethyl]-2,3-dihydro-4(1H)-quinazolinone

Guidance literature:: With sodium hydride; In N,N-dimethyl acetamide; for 3h; Ambient temperature;

Reference yield: 85.0%

: 159794-16-8
6-chloro-1-cyclohexylmethyl-3-[2-(diethylamino)ethyl]-2,3-dihydro-4(1H)-quinazolinone

Guidance literature:

Reference yield:

: 4743-17-3
5-Chloroisatoic anhydride

: 159794-16-8
6-chloro-1-cyclohexylmethyl-3-[2-(diethylamino)ethyl]-2,3-dihydro-4(1H)-quinazolinone

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / dioxane / 2 h / 60 °C

2: 2.) 80percent w/v NaOH / 1.) ethanol/water, reflux, 1 h; 2.) ethanol/water, reflux, 20 min

3: 85 percent / sodium hydride / N,N-dimethyl-acetamide / 3 h / Ambient temperature

With sodium hydroxide; sodium hydride; In 1,4-dioxane; N,N-dimethyl acetamide;