2-Amino-5-chloro-N-[2-(diethylamino)ethyl]benzamide

Base Information

Chemical Name:2-Amino-5-chloro-N-[2-(diethylamino)ethyl]benzamide
CAS No.:30646-50-5
Molecular Formula:C₁₃H₂₀ClN₃O
Molecular Weight:269.774
Hs Code.:
DSSTox Substance ID:DTXSID701225577

Synonyms:2-Amino-5-chloro-N(2-diethylaminoethyl)benzamide;SCHEMBL8771439;2-AMINO-5-CHLORO-N-[2-(DIETHYLAMINO)ETHYL]BENZAMIDE;DTXSID701225577;AKOS000145375;30646-50-5

Suppliers and Price of 2-Amino-5-chloro-N-[2-(diethylamino)ethyl]benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Amino-5-chloro-N-[2-(diethylamino)ethyl]benzamide

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:269.1294900
Heavy Atom Count:18
Complexity:259

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCN(CC)CCNC(=O)C1=C(C=CC(=C1)Cl)N

Technology Process of 2-Amino-5-chloro-N-[2-(diethylamino)ethyl]benzamide

There total 2 articles about 2-Amino-5-chloro-N-[2-(diethylamino)ethyl]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 4743-17-3
5-Chloroisatoic anhydride

: 100-36-7
N,N-diethylethylenediamine

: 30646-50-5
2-amino-5-chloro-N-[2-(diethylamino)ethyl] benzamide

Guidance literature:: In 1,4-dioxane; at 60 ℃; for 2h;

Reference yield: 76.0%

: 30646-50-5
2-amino-5-chloro-N-[2-(diethylamino)ethyl] benzamide

Guidance literature:

Reference yield:

: 30646-50-5
2-amino-5-chloro-N-[2-(diethylamino)ethyl] benzamide

: 6-Chloro-1-cyclohexylmethyl-3-[2-(diethylamino)ethyl]-2,3-dihydro-4(1H)-quinazolinone citrate

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) 80percent w/v NaOH / 1.) ethanol/water, reflux, 1 h; 2.) ethanol/water, reflux, 20 min

2: 85 percent / sodium hydride / N,N-dimethyl-acetamide / 3 h / Ambient temperature

3: ethanol; diethyl ether

With sodium hydroxide; sodium hydride; In diethyl ether; ethanol; N,N-dimethyl acetamide;