Technology Process of C17H18N2O3S
There total 6 articles about C17H18N2O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C13H12N2OS;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 20 ℃;
for 0.75h;
chloroacetic acid ethyl ester;
In
N,N-dimethyl-formamide; mineral oil;
for 2h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 2 h / 90 °C
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 20 °C
2.2: 2 h
With
tetrakis(triphenylphosphine) palladium(0); sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 3-chloro-benzenecarboperoxoic acid / ethanol / 3 h / Reflux
2.1: water; sodium hydroxide / tetrahydrofuran; methanol / 16 h / 40 °C
3.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
3.2: 1 h / 20 °C
4.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 2 h / 20 °C
4.2: 1 h / 20 °C
5.1: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 2 h / 90 °C
6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 20 °C
6.2: 2 h
With
tetrakis(triphenylphosphine) palladium(0); n-butyllithium; oxalyl dichloride; water; sodium hydride; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
