Technology Process of C17H28O2Sn
There total 5 articles about C17H28O2Sn which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); hexamethyldistannane; lithium chloride;
In
tetrahydrofuran;
at 70 ℃;
DOI:10.1246/bcsj.20120152
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-methylcyclohexylamine; isobutyl chloroformate / dichloromethane / -15 °C
2: tetrahydrofuran / 0 °C
3: potassium hexamethylsilazane; N,N-phenylbistrifluoromethane-sulfonimide / tetrahydrofuran / -78 °C
4: lithium chloride; hexamethyldistannane; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 70 °C
With
N-methylcyclohexylamine; tetrakis(triphenylphosphine) palladium(0); N,N-phenylbistrifluoromethane-sulfonimide; hexamethyldistannane; potassium hexamethylsilazane; lithium chloride; isobutyl chloroformate;
In
tetrahydrofuran; dichloromethane;
4: |Stille Cross Coupling;
DOI:10.1246/bcsj.20120152
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: pivaloyl chloride; triethylamine / tetrahydrofuran / -20 °C
1.2: -20 - 20 °C
2.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C
2.2: -78 - 40 °C
3.1: lithium hydroxide; dihydrogen peroxide / tetrahydrofuran; water / 0 - 20 °C
4.1: N-methylcyclohexylamine; isobutyl chloroformate / dichloromethane / -15 °C
5.1: tetrahydrofuran / 0 °C
6.1: potassium hexamethylsilazane; N,N-phenylbistrifluoromethane-sulfonimide / tetrahydrofuran / -78 °C
7.1: lithium chloride; hexamethyldistannane; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 70 °C
With
N-methylcyclohexylamine; tetrakis(triphenylphosphine) palladium(0); N,N-phenylbistrifluoromethane-sulfonimide; dihydrogen peroxide; hexamethyldistannane; sodium hexamethyldisilazane; pivaloyl chloride; potassium hexamethylsilazane; triethylamine; lithium chloride; lithium hydroxide; isobutyl chloroformate;
In
tetrahydrofuran; dichloromethane; water;
7.1: |Stille Cross Coupling;
DOI:10.1246/bcsj.20120152