{2-[5-(4-benzyloxyphenyl)-6-butylpyridazin-3-yloxy]-ethyl} diethylamine

Base Information

Chemical Name:{2-[5-(4-benzyloxyphenyl)-6-butylpyridazin-3-yloxy]-ethyl} diethylamine
CAS No.:1331775-19-9
Molecular Formula:C₂₇H₃₅N₃O₂
Molecular Weight:433.594
Hs Code.:

Synonyms:{2-[5-(4-benzyloxyphenyl)-6-butylpyridazin-3-yloxy]-ethyl} diethylamine

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Chemical Property of {2-[5-(4-benzyloxyphenyl)-6-butylpyridazin-3-yloxy]-ethyl} diethylamine

Chemical Property:

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Technology Process of {2-[5-(4-benzyloxyphenyl)-6-butylpyridazin-3-yloxy]-ethyl} diethylamine

There total 4 articles about {2-[5-(4-benzyloxyphenyl)-6-butylpyridazin-3-yloxy]-ethyl} diethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1331775-12-2
4-(4-benzyloxyphenyl)-3-butyl-6-chloropyridazine

: 100-37-8
2-(Diethylamino)ethanol

: 1331775-19-9
{2-[5-(4-benzyloxyphenyl)-6-butylpyridazin-3-yloxy]-ethyl} diethylamine

Guidance literature:: 2-(Diethylamino)ethanol; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.166667h;

4-(4-benzyloxyphenyl)-3-butyl-6-chloropyridazine; In tetrahydrofuran; at 50 - 55 ℃;

Reference yield:

: 243641-09-0
2-[4-(Benzyloxy)phenyl]-N-methoxy-N-methylacetamide

: 1331775-19-9
{2-[5-(4-benzyloxyphenyl)-6-butylpyridazin-3-yloxy]-ethyl} diethylamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrahydrofuran / 0.5 h / -10 - 20 °C

1.2: 0 °C

2.1: triethylamine / toluene / 16 h / 20 °C

3.1: hydrazine hydrate / acetic acid / 4 h / 120 °C

4.1: trichlorophosphate / 2 h / 70 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C

5.2: 50 - 55 °C

With sodium hydride; hydrazine hydrate; triethylamine; trichlorophosphate; In tetrahydrofuran; acetic acid; toluene; mineral oil;

Reference yield:

: 1331775-09-7
1-(4-benzyloxyphenyl)hexan-2-one

: 1331775-19-9
{2-[5-(4-benzyloxyphenyl)-6-butylpyridazin-3-yloxy]-ethyl} diethylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / toluene / 16 h / 20 °C

2.1: hydrazine hydrate / acetic acid / 4 h / 120 °C

3.1: trichlorophosphate / 2 h / 70 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C

4.2: 50 - 55 °C

With sodium hydride; hydrazine hydrate; triethylamine; trichlorophosphate; In tetrahydrofuran; acetic acid; toluene; mineral oil;