(2S,3R,4S,5R)-4-Benzyloxy-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-ol

Base Information

Chemical Name:(2S,3R,4S,5R)-4-Benzyloxy-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-ol
CAS No.:1064180-95-5
Molecular Formula:C₁₃H₁₈O₄
Molecular Weight:238.284
Hs Code.:

Synonyms:(2S,3R,4S,5R)-4-Benzyloxy-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-ol

Suppliers and Price of (2S,3R,4S,5R)-4-Benzyloxy-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R,4S,5R)-4-Benzyloxy-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-ol

Chemical Property:

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Technology Process of (2S,3R,4S,5R)-4-Benzyloxy-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-ol

There total 6 articles about (2S,3R,4S,5R)-4-Benzyloxy-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 445299-17-2
2,6-anhydro-4-O-benzyl-1-deoxy-1-phenylsulfanyl-β-D-fructopyranoside

: 1064180-95-5
(2S,3R,4S,5R)-4-Benzyloxy-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-ol

: (2R,3R,4S,5R)-4-Benzyloxy-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-ol

: 445299-18-3
(1R,4R,5S,6S)-5-Benzyloxy-1-methyl-2,7-dioxa-bicyclo[2.2.1]heptan-6-ol

Guidance literature:: With nickel; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/S0040-4020(02)00233-8

Reference yield:

: 1064180-91-1
C₁₃H₁₇IO₄

: 1064180-95-5
(2S,3R,4S,5R)-4-Benzyloxy-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1021/jo8013534

Reference yield:

: 100-39-0
benzyl bromide

: 1064180-95-5
(2S,3R,4S,5R)-4-Benzyloxy-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: Bu₂SnO / methanol / 4 h / Heating

1.2: 58 percent / CsF / dimethylformamide / 17 h / 20 °C

2.1: 85 percent / (Bu₃Sn)2O; 4 Angstroem molecular sieves / various solvent(s) / 5 h / Heating

3.1: Raney nickel / tetrahydrofuran / 20 °C

With 4 A molecular sieve; nickel; di(n-butyl)tin oxide; bis(tri-n-butyltin)oxide; In tetrahydrofuran; methanol;
DOI:10.1016/S0040-4020(02)00233-8