9,9-Bis-(2,4,6-trimethyl-phenyl)-8b,9-dihydro-4bH-9-sila-benzo[3,4]cyclobuta[1,2-a]indene

Base Information

• Chemical Name: 9,9-Bis-(2,4,6-trimethyl-phenyl)-8b,9-dihydro-4bH-9-sila-benzo[3,4]cyclobuta[1,2-a]indene
• CAS No.: 109828-73-1
• Molecular Formula: C₃₂H₃₂Si
• Molecular Weight: 444.692
• Mol file: 109828-73-1.mol

Synonyms:9,9-Bis-(2,4,6-trimethyl-phenyl)-8b,9-dihydro-4bH-9-sila-benzo[3,4]cyclobuta[1,2-a]indene

Chemical Property of 9,9-Bis-(2,4,6-trimethyl-phenyl)-8b,9-dihydro-4bH-9-sila-benzo[3,4]cyclobuta[1,2-a]indene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9,9-Bis-(2,4,6-trimethyl-phenyl)-8b,9-dihydro-4bH-9-sila-benzo[3,4]cyclobuta[1,2-a]indene

There total 5 articles about 9,9-Bis-(2,4,6-trimethyl-phenyl)-8b,9-dihydro-4bH-9-sila-benzo[3,4]cyclobuta[1,2-a]indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

C32H32Si (109828-65-1) → anthracene (120-12-7) + 9,9-Bis-(2,4,6-trimethyl-phenyl)-8b,9-dihydro-4bH-9-sila-benzo[3,4]cyclobuta[1,2-a]indene (109828-73-1) + C32H32Si

Guidance literature:

With 9,10-dibenzoanthracene; In dichloromethane; Product distribution; Irradiation; other solvent;

DOI:10.1016/0040-4039(95)01263-H

Reference yield: 28.0%

C32H32Si (109828-65-1) + 2,3-dimethyl-buta-1,3-diene (513-81-5) → 9,9-Bis-(2,4,6-trimethyl-phenyl)-8b,9-dihydro-4bH-9-sila-benzo[3,4]cyclobuta[1,2-a]indene (109828-73-1)

Guidance literature:

In cyclohexane; Irradiation;

DOI:10.1246/cl.1986.1797

Reference yield:

C32H32Si (109828-65-1) → anthracene (120-12-7) + 9,9-Bis-(2,4,6-trimethyl-phenyl)-8b,9-dihydro-4bH-9-sila-benzo[3,4]cyclobuta[1,2-a]indene (109828-73-1) + C32H32Si

Guidance literature:

With 9,10-Dicyanoanthracene; In dichloromethane; for 3h; Irradiation;

DOI:10.1016/S0040-4020(96)01076-9

upstream raw materials:

C₃₂H₃₂Si

2,3-dimethyl-buta-1,3-diene

ethenetetracarbonitrile

lithium anthracenide