N,N-bis(ethoxycarbonylmethyl)-2-(ethoxycarbonylmethoxy)-5-aminobenzylamine

Base Information

Chemical Name:N,N-bis(ethoxycarbonylmethyl)-2-(ethoxycarbonylmethoxy)-5-aminobenzylamine
CAS No.:308124-32-5
Molecular Formula:C₁₉H₂₈N₂O₇
Molecular Weight:396.441
Hs Code.:

Synonyms:N,N-bis(ethoxycarbonylmethyl)-2-(ethoxycarbonylmethoxy)-5-aminobenzylamine

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Chemical Property of N,N-bis(ethoxycarbonylmethyl)-2-(ethoxycarbonylmethoxy)-5-aminobenzylamine

Chemical Property:

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Technology Process of N,N-bis(ethoxycarbonylmethyl)-2-(ethoxycarbonylmethoxy)-5-aminobenzylamine

There total 5 articles about N,N-bis(ethoxycarbonylmethyl)-2-(ethoxycarbonylmethoxy)-5-aminobenzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 308124-31-4
N,N-bis(ethoxycarbonylmethyl)-2-(ethoxycarbonylmethoxy)-5-nitrobenzylamine

: 308124-32-5
N,N-bis(ethoxycarbonylmethyl)-2-(ethoxycarbonylmethoxy)-5-aminobenzylamine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; under 2585.81 - 3102.97 Torr;

Reference yield:

: 932-30-9
2-Hydroxybenzylamine

: 308124-32-5
N,N-bis(ethoxycarbonylmethyl)-2-(ethoxycarbonylmethoxy)-5-aminobenzylamine

Guidance literature:: Multi-step reaction with 4 steps

1: KI; Na₂HPO₄ / acetonitrile / Heating

2: 6.8 g / K₂CO₃; 3A molecular sieves / acetonitrile / 24 h / Heating

3: 72 percent / aq. HNO₃; AcOH

4: 94 percent / H₂ / Pd/C / ethanol / 2585.81 - 3102.97 Torr

With disodium hydrogenphosphate; 3 A molecular sieve; hydrogen; nitric acid; potassium carbonate; acetic acid; potassium iodide; palladium on activated charcoal; In ethanol; acetonitrile; 1: Alkylation / 2: Etherification / 3: Nitration / 4: Reduction;

Reference yield:

: 308124-30-3
N,N-bis(ethoxycarbonylmethyl)-2-(ethoxycarbonylmethoxy)-benzylamine

: 308124-32-5
N,N-bis(ethoxycarbonylmethyl)-2-(ethoxycarbonylmethoxy)-5-aminobenzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / aq. HNO₃; AcOH

2: 94 percent / H₂ / Pd/C / ethanol / 2585.81 - 3102.97 Torr

With hydrogen; nitric acid; acetic acid; palladium on activated charcoal; In ethanol; 1: Nitration / 2: Reduction;