(2E,4E)-(R)-10-(tert-Butyl-diphenyl-silanyloxy)-7-methyl-deca-2,4-dienoic acid ethyl ester

Base Information

Chemical Name:(2E,4E)-(R)-10-(tert-Butyl-diphenyl-silanyloxy)-7-methyl-deca-2,4-dienoic acid ethyl ester
CAS No.:342374-97-4
Molecular Formula:C₂₉H₄₀O₃Si
Molecular Weight:464.72
Hs Code.:

Synonyms:(2E,4E)-(R)-10-(tert-Butyl-diphenyl-silanyloxy)-7-methyl-deca-2,4-dienoic acid ethyl ester

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Chemical Property of (2E,4E)-(R)-10-(tert-Butyl-diphenyl-silanyloxy)-7-methyl-deca-2,4-dienoic acid ethyl ester

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Technology Process of (2E,4E)-(R)-10-(tert-Butyl-diphenyl-silanyloxy)-7-methyl-deca-2,4-dienoic acid ethyl ester

There total 4 articles about (2E,4E)-(R)-10-(tert-Butyl-diphenyl-silanyloxy)-7-methyl-deca-2,4-dienoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 31930-36-6,31930-37-7
ethyl (E)-3-iodopropenoate

: C₃₀H₄₇BO₃Si

: 342374-97-4
(2E,4E)-(R)-10-(tert-Butyl-diphenyl-silanyloxy)-7-methyl-deca-2,4-dienoic acid ethyl ester

Guidance literature:: With sodium hydroxide; triphenylphosphine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In tetrahydrofuran; water; Heating;
DOI:10.1016/S0040-4039(01)00217-9

Reference yield:

: 2385-77-5
(R)-Citronellal

: 342374-97-4
(2E,4E)-(R)-10-(tert-Butyl-diphenyl-silanyloxy)-7-methyl-deca-2,4-dienoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

2: 86 percent / chromous chloride; LiI / tetrahydrofuran

3: 87 percent / Ph₃P; NaOH / Pd₂((dba)2*CHCl₃ / tetrahydrofuran; H₂O / Heating

With chromium dichloride; sodium hydroxide; triphenylphosphine; lithium iodide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In tetrahydrofuran; water; 3: Suzuki coupling;
DOI:10.1016/S0040-4039(01)00217-9

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 342374-97-4
(2E,4E)-(R)-10-(tert-Butyl-diphenyl-silanyloxy)-7-methyl-deca-2,4-dienoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

2: 86 percent / chromous chloride; LiI / tetrahydrofuran

3: 87 percent / Ph₃P; NaOH / Pd₂((dba)2*CHCl₃ / tetrahydrofuran; H₂O / Heating

With chromium dichloride; sodium hydroxide; triphenylphosphine; lithium iodide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In tetrahydrofuran; water; 3: Suzuki coupling;
DOI:10.1016/S0040-4039(01)00217-9