3,5-dichloro-N-((2,3-dihydropyrazolo[5,1-b]oxazol-6-yl)methyl)-N-methylaniline

Base Information

Chemical Name:3,5-dichloro-N-((2,3-dihydropyrazolo[5,1-b]oxazol-6-yl)methyl)-N-methylaniline
CAS No.:1427462-02-9
Molecular Formula:C₁₃H₁₃Cl₂N₃O
Molecular Weight:298.172
Hs Code.:

Synonyms:3,5-dichloro-N-((2,3-dihydropyrazolo[5,1-b]oxazol-6-yl)methyl)-N-methylaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-dichloro-N-((2,3-dihydropyrazolo[5,1-b]oxazol-6-yl)methyl)-N-methylaniline

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Technology Process of 3,5-dichloro-N-((2,3-dihydropyrazolo[5,1-b]oxazol-6-yl)methyl)-N-methylaniline

There total 4 articles about 3,5-dichloro-N-((2,3-dihydropyrazolo[5,1-b]oxazol-6-yl)methyl)-N-methylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1427462-01-8
C₂₀H₂₁Cl₂N₃O₄S

: 1427462-02-9
3,5-dichloro-N-((2,3-dihydropyrazolo[5,1-b]oxazol-6-yl)methyl)-N-methylaniline

Guidance literature:: With sodium hydride; In acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1021/jm400079a

Reference yield:

: 42266-03-5
3,5-dichloro-N-methylaniline

: 1427462-02-9
3,5-dichloro-N-((2,3-dihydropyrazolo[5,1-b]oxazol-6-yl)methyl)-N-methylaniline

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate; sodium iodide / acetonitrile

2: ethanol / 20 °C

3: triethylamine / acetonitrile / 0.33 h

4: sodium hydride / acetonitrile / 20 °C / Inert atmosphere

With sodium hydride; sodium hydrogencarbonate; triethylamine; sodium iodide; In ethanol; acetonitrile;
DOI:10.1021/jm400079a

Reference yield:

: C₁₃H₁₅Cl₂N₃O₂

: 1427462-02-9
3,5-dichloro-N-((2,3-dihydropyrazolo[5,1-b]oxazol-6-yl)methyl)-N-methylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / acetonitrile / 0.33 h

2: sodium hydride / acetonitrile / 20 °C / Inert atmosphere

With sodium hydride; triethylamine; In acetonitrile;
DOI:10.1021/jm400079a