5-(((3,5-dichlorophenyl)(methyl)amino)methyl)-1-methyl-2-vinyl-1H-pyrazol-3(2H)-one

Base Information

Chemical Name:5-(((3,5-dichlorophenyl)(methyl)amino)methyl)-1-methyl-2-vinyl-1H-pyrazol-3(2H)-one
CAS No.:1427462-03-0
Molecular Formula:C₁₄H₁₅Cl₂N₃O
Molecular Weight:312.199
Hs Code.:

Synonyms:5-(((3,5-dichlorophenyl)(methyl)amino)methyl)-1-methyl-2-vinyl-1H-pyrazol-3(2H)-one

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Chemical Property of 5-(((3,5-dichlorophenyl)(methyl)amino)methyl)-1-methyl-2-vinyl-1H-pyrazol-3(2H)-one

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Technology Process of 5-(((3,5-dichlorophenyl)(methyl)amino)methyl)-1-methyl-2-vinyl-1H-pyrazol-3(2H)-one

There total 5 articles about 5-(((3,5-dichlorophenyl)(methyl)amino)methyl)-1-methyl-2-vinyl-1H-pyrazol-3(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1427462-02-9
3,5-dichloro-N-((2,3-dihydropyrazolo[5,1-b]oxazol-6-yl)methyl)-N-methylaniline

: 333-27-7
methyl trifluoromethanesulfonate

: 1427462-03-0
5-(((3,5-dichlorophenyl)(methyl)amino)methyl)-1-methyl-2-vinyl-1H-pyrazol-3(2H)-one

Guidance literature:: 3,5-dichloro-N-((2,3-dihydropyrazolo[5,1-b]oxazol-6-yl)methyl)-N-methylaniline; methyl trifluoromethanesulfonate; In acetonitrile; at 20 ℃; for 2h;

With toluene-4-sulfonic acid; sodium iodide; In acetonitrile;

With potassium tert-butylate; In acetonitrile; for 1h;
DOI:10.1021/jm400079a

Reference yield:

: 1427462-01-8
C₂₀H₂₁Cl₂N₃O₄S

: 1427462-03-0
5-(((3,5-dichlorophenyl)(methyl)amino)methyl)-1-methyl-2-vinyl-1H-pyrazol-3(2H)-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / acetonitrile / 20 °C / Inert atmosphere

2.1: acetonitrile / 2 h / 20 °C

2.3: 1 h

With sodium hydride; In acetonitrile;
DOI:10.1021/jm400079a

Reference yield:

: 42266-03-5
3,5-dichloro-N-methylaniline

: 1427462-03-0
5-(((3,5-dichlorophenyl)(methyl)amino)methyl)-1-methyl-2-vinyl-1H-pyrazol-3(2H)-one

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydrogencarbonate; sodium iodide / acetonitrile

2.1: ethanol / 20 °C

3.1: triethylamine / acetonitrile / 0.33 h

4.1: sodium hydride / acetonitrile / 20 °C / Inert atmosphere

5.1: acetonitrile / 2 h / 20 °C

5.3: 1 h

With sodium hydride; sodium hydrogencarbonate; triethylamine; sodium iodide; In ethanol; acetonitrile;
DOI:10.1021/jm400079a