4-(3,4-Dichloro-phenyl)-2-(3,4,4-trimethyl-2-thioxo-thiazolidin-5-yl)-[1,2,4]oxadiazolidine-3,5-dione

Base Information

Chemical Name:4-(3,4-Dichloro-phenyl)-2-(3,4,4-trimethyl-2-thioxo-thiazolidin-5-yl)-[1,2,4]oxadiazolidine-3,5-dione
CAS No.:132373-06-9
Molecular Formula:C₁₄H₁₃Cl₂N₃O₃S₂
Molecular Weight:406.314
Hs Code.:

Synonyms:4-(3,4-Dichloro-phenyl)-2-(3,4,4-trimethyl-2-thioxo-thiazolidin-5-yl)-[1,2,4]oxadiazolidine-3,5-dione

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Chemical Property of 4-(3,4-Dichloro-phenyl)-2-(3,4,4-trimethyl-2-thioxo-thiazolidin-5-yl)-[1,2,4]oxadiazolidine-3,5-dione

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Technology Process of 4-(3,4-Dichloro-phenyl)-2-(3,4,4-trimethyl-2-thioxo-thiazolidin-5-yl)-[1,2,4]oxadiazolidine-3,5-dione

There total 1 articles about 4-(3,4-Dichloro-phenyl)-2-(3,4,4-trimethyl-2-thioxo-thiazolidin-5-yl)-[1,2,4]oxadiazolidine-3,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 116121-36-9
C₁₃H₁₅Cl₂N₃O₂S₂

: 79-22-1
methyl chloroformate

: 132373-06-9
4-(3,4-Dichloro-phenyl)-2-(3,4,4-trimethyl-2-thioxo-thiazolidin-5-yl)-[1,2,4]oxadiazolidine-3,5-dione

Guidance literature:: With triethylamine; In acetone;
DOI:10.1007/BF00509717

Reference yield:

: 132373-06-9
4-(3,4-Dichloro-phenyl)-2-(3,4,4-trimethyl-2-thioxo-thiazolidin-5-yl)-[1,2,4]oxadiazolidine-3,5-dione

: 2327-02-8
3,4-dichlorophenylurea

Guidance literature:: Multi-step reaction with 2 steps

1: MeOCOCl, Et₃N

2: conc. HCl / ethanol; H₂O / Heating

With hydrogenchloride; triethylamine; methyl chloroformate; In ethanol; water;
DOI:10.1007/BF00509717

Reference yield:

: 132373-06-9
4-(3,4-Dichloro-phenyl)-2-(3,4,4-trimethyl-2-thioxo-thiazolidin-5-yl)-[1,2,4]oxadiazolidine-3,5-dione

: 116121-50-7
1-(3,4-Dichloro-phenyl)-3-(3,5,5-trimethyl-2-thioxo-thiazolidin-4-yl)-urea

Guidance literature:: Multi-step reaction with 3 steps

1: MeOCOCl, Et₃N

2: conc. HCl / ethanol; H₂O / Heating

3: 56 percent / p-TsOH / benzene / Heating; or toluene

With hydrogenchloride; toluene-4-sulfonic acid; triethylamine; methyl chloroformate; In ethanol; water; benzene;
DOI:10.1007/BF00509717