2-hydroxy-3-methyl-6-non-1-ynyl-4-(tetrahydro-pyran-2-yloxy)-benzaldehyde

Base Information

Chemical Name:2-hydroxy-3-methyl-6-non-1-ynyl-4-(tetrahydro-pyran-2-yloxy)-benzaldehyde
CAS No.:859507-92-9
Molecular Formula:C₂₂H₃₀O₄
Molecular Weight:358.478
Hs Code.:

Synonyms:2-hydroxy-3-methyl-6-non-1-ynyl-4-(tetrahydro-pyran-2-yloxy)-benzaldehyde

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Chemical Property of 2-hydroxy-3-methyl-6-non-1-ynyl-4-(tetrahydro-pyran-2-yloxy)-benzaldehyde

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Technology Process of 2-hydroxy-3-methyl-6-non-1-ynyl-4-(tetrahydro-pyran-2-yloxy)-benzaldehyde

There total 1 articles about 2-hydroxy-3-methyl-6-non-1-ynyl-4-(tetrahydro-pyran-2-yloxy)-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 859507-78-1
2,4-dihydroxy-3-methyl-6-non-1-ynyl-benzaldehyde

: 859507-92-9
2-hydroxy-3-methyl-6-non-1-ynyl-4-(tetrahydro-pyran-2-yloxy)-benzaldehyde

Guidance literature:: With pyridinium p-toluenesulfonate; In benzene; at 60 ℃; for 15h;
DOI:10.1021/ja052049g

Reference yield:

: 859507-92-9
2-hydroxy-3-methyl-6-non-1-ynyl-4-(tetrahydro-pyran-2-yloxy)-benzaldehyde

: 74-88-4
methyl iodide

: 2-methoxy-3-methyl-6-non-1-ynyl-4-(tetrahydro-pyran-2-yloxy)-benzaldehyde

Guidance literature:: 2-hydroxy-3-methyl-6-non-1-ynyl-4-(tetrahydro-pyran-2-yloxy)-benzaldehyde; With ISOPROPYLAMIDE; sodium hydride; In tetrahydrofuran; at 0 - 20 ℃;

methyl iodide; In tetrahydrofuran; at 60 ℃; for 9h;
DOI:10.1021/ja052049g

Reference yield:

: 859507-92-9
2-hydroxy-3-methyl-6-non-1-ynyl-4-(tetrahydro-pyran-2-yloxy)-benzaldehyde

: 859507-80-5
4-hydroxy-2-methoxy-3-methyl-6-non-1-ynyl-benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH; dimethylacetamide / tetrahydrofuran / 0 - 20 °C

1.2: tetrahydrofuran / 9 h / 60 °C

2.1: 280 mg / aq. HCl / methanol / 0.33 h / 20 °C

With hydrogenchloride; ISOPROPYLAMIDE; sodium hydride; In tetrahydrofuran; methanol;
DOI:10.1021/ja052049g