(S)-2-(Carboxymethyl-amino)-3-phenyl-propionic acid benzyl ester; hydrochloride

Base Information

• Chemical Name: (S)-2-(Carboxymethyl-amino)-3-phenyl-propionic acid benzyl ester; hydrochloride
• CAS No.: 128684-56-0
• Molecular Formula: C₁₈H₁₉NO₄*ClH
• Molecular Weight: 349.814

Synonyms:(S)-2-(Carboxymethyl-amino)-3-phenyl-propionic acid benzyl ester; hydrochloride

Chemical Property of (S)-2-(Carboxymethyl-amino)-3-phenyl-propionic acid benzyl ester; hydrochloride

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Technology Process of (S)-2-(Carboxymethyl-amino)-3-phenyl-propionic acid benzyl ester; hydrochloride

There total 4 articles about (S)-2-(Carboxymethyl-amino)-3-phenyl-propionic acid benzyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-2-(tert-Butoxycarbonylmethyl-amino)-3-phenyl-propionic acid benzyl ester → (R)-2-(Carboxymethyl-amino)-3-phenyl-propionic acid benzyl ester; hydrochloride (128684-56-0)

Guidance literature:

With hydrogenchloride; In ethyl acetate; for 2h; Ambient temperature;

DOI:10.1021/jm00171a034

Reference yield:

(S)-benzyl 2-(2-tert-butoxy-2-oxoethylamino)-3-phenylpropanoate (254974-59-9) → (S)-2-(Carboxymethyl-amino)-3-phenyl-propionic acid benzyl ester; hydrochloride (128684-56-0)

Guidance literature:

With hydrogenchloride; In ethyl acetate; for 2h; Ambient temperature;

DOI:10.1021/jm00171a034

Reference yield:

L-Phenylalanine benzyl ester (962-39-0) → (S)-2-(Carboxymethyl-amino)-3-phenyl-propionic acid benzyl ester; hydrochloride (128684-56-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 92.8 percent / triethylamine / tetrahydrofuran / 96 h

2: 2N HCl / ethyl acetate / 2 h / Ambient temperature

With hydrogenchloride; triethylamine; In tetrahydrofuran; ethyl acetate;

DOI:10.1021/jm00171a034

upstream raw materials:

D-phenylalanine benzyl ester

(S)-benzyl 2-(2-tert-butoxy-2-oxoethylamino)-3-phenylpropanoate

L-Phenylalanine benzyl ester

Downstream raw materials:

(R)-2-[({(S)-5-((R)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-5-[(R)-2-(1H-indol-3-yl)-1-(3-methyl-butylcarbamoyl)-ethylcarbamoyl]-pentylcarbamoyl}-methyl)-amino]-3-phenyl-propionic acid benzyl ester

(5R,8R,11S)-5,8-Dibenzyl-2,6,9-trioxo-1,4,7,10-tetraaza-cyclopentadecane-11-carboxylic acid [(R)-2-(1H-indol-3-yl)-1-(3-methyl-butylcarbamoyl)-ethyl]-amide

(3R,8R,11S)-3,8-Dibenzyl-2,6,9-trioxo-1,4,7,10-tetraaza-cyclopentadecane-11-carboxylic acid [(R)-2-(1H-indol-3-yl)-1-(3-methyl-butylcarbamoyl)-ethyl]-amide

(R)-2-{[((R)-1-{(S)-5-Amino-1-[(R)-2-(1H-indol-3-yl)-1-(3-methyl-butylcarbamoyl)-ethylcarbamoyl]-pentylcarbamoyl}-2-phenyl-ethylcarbamoyl)-methyl]-amino}-3-phenyl-propionic acid

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