C₂₉H₂₅ClN₂O₅

Base Information

Chemical Name:C₂₉H₂₅ClN₂O₅
CAS No.:1265630-54-3
Molecular Formula:C₂₉H₂₅ClN₂O₅
Molecular Weight:516.981
Hs Code.:

C<sub>29</sub>H<sub>25</sub>ClN<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₉H₂₅ClN₂O₅

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Chemical Property of C₂₉H₂₅ClN₂O₅

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Technology Process of C₂₉H₂₅ClN₂O₅

There total 13 articles about C₂₉H₂₅ClN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1423689-66-0
C₃₀H₂₇ClN₂O₅

: 1265630-54-3
C₂₉H₂₅ClN₂O₅

Guidance literature:: C₃₀H₂₇ClN₂O₅; With lithium hydroxide monohydrate; water; In methanol; at 20 ℃;

With hydrogenchloride; In water; pH=4 - 5;

Reference yield:

: 2142-68-9
1-(2-chlorophenyl)ethanone

: 1265630-54-3
C₂₉H₂₅ClN₂O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; dimethylsulfide borane complex / tetrahydrofuran / 0.5 h / 20 °C

2.1: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 80 °C

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 90 °C / Inert atmosphere

4.1: water; lithium hydroxide monohydrate / methanol / 20 °C

4.2: pH 4 - 5

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; lithium hydroxide monohydrate; dimethylsulfide borane complex; diphenyl phosphoryl azide; water; sodium carbonate; triethylamine; (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; toluene;

Reference yield:

: 29203-58-5
4-bromo-N-hydroxybenzenecarboximidoyl chloride

: 1265630-54-3
C₂₉H₂₅ClN₂O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium methylate / methanol / 0.67 h / 0 - 25 °C

2.1: water; sodium hydroxide / tetrahydrofuran / 3 h / 20 °C

2.2: pH Ca_. 3 / Cooling with ice

3.1: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 80 °C

4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 90 °C / Inert atmosphere

5.1: water; lithium hydroxide monohydrate / methanol / 20 °C

5.2: pH 4 - 5

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; lithium hydroxide monohydrate; diphenyl phosphoryl azide; water; sodium methylate; sodium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; toluene;