3-(3-chloropropox y)-N-(3,5-dichloropyridin-4-yl) - 4-methoxybenzamine

Base Information

Chemical Name:3-(3-chloropropox y)-N-(3,5-dichloropyridin-4-yl) - 4-methoxybenzamine
CAS No.:1185160-66-0
Molecular Formula:C₁₆H₁₅Cl₃N₂O₃
Molecular Weight:389.666
Hs Code.:

Synonyms:3-(3-chloropropox y)-N-(3,5-dichloropyridin-4-yl) - 4-methoxybenzamine

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Chemical Property of 3-(3-chloropropox y)-N-(3,5-dichloropyridin-4-yl) - 4-methoxybenzamine

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Technology Process of 3-(3-chloropropox y)-N-(3,5-dichloropyridin-4-yl) - 4-methoxybenzamine

There total 7 articles about 3-(3-chloropropox y)-N-(3,5-dichloropyridin-4-yl) - 4-methoxybenzamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22889-78-7
3,5-dichloro-4-aminopyridine

: 3-(3-chloropropoxy)-4-methoxybenzoic acid

: 1185160-66-0
3-(3-chloropropox y)-N-(3,5-dichloropyridin-4-yl) - 4-methoxybenzamine

Guidance literature:: 3,5-dichloro-4-aminopyridine; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 30 ℃; for 3h;

3-(3-chloropropoxy)-4-methoxybenzoic acid; With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; mineral oil; at 0 - 30 ℃; for 1.25h;

Reference yield:

: 22889-78-7
3,5-dichloro-4-aminopyridine

: 1609152-85-3
C₁₁H₁₂Cl₂O₃

: 1185160-66-0
3-(3-chloropropox y)-N-(3,5-dichloropyridin-4-yl) - 4-methoxybenzamine

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 15 - 25 ℃; for 5h;
DOI:10.3184/174751913X13782291519608

Reference yield:

: 645-08-9,74309-78-7
Isovanillic acid

: 1185160-66-0
3-(3-chloropropox y)-N-(3,5-dichloropyridin-4-yl) - 4-methoxybenzamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 50 °C

1.2: 2 h / 20 °C

1.3: pH 7

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / 30 °C

2.2: 1.25 h / 0 - 30 °C

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; mineral oil;