C₂₇H₃₀N₂O₄

Base Information

Chemical Name:C₂₇H₃₀N₂O₄
CAS No.:132143-02-3
Molecular Formula:C₂₇H₃₀N₂O₄
Molecular Weight:446.546
Hs Code.:

C<sub>27</sub>H<sub>30</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₇H₃₀N₂O₄

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Chemical Property of C₂₇H₃₀N₂O₄

Chemical Property:

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Technology Process of C₂₇H₃₀N₂O₄

There total 13 articles about C₂₇H₃₀N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58594-50-6
3-(2'-nitrophenyl)pyrrolidine-2,5-dione

: 132143-02-3
C₂₇H₃₀N₂O₄

Guidance literature:: Multi-step reaction with 11 steps

1: Et₃N / DMAP / CH₂Cl₂ / 0 deg C to room temperature

2: 95 percent / H₂ / 10percent Pd/C / toluene; ethanol / 18 h / 760 Torr

3: toluene / Ambient temperature

4: 1.5 M n-BuLi / 2-methyl-propan-2-ol; tetrahydrofuran; hexane; toluene / 0.5 h / 5 °C

5: toluene

6: 20percent aq. HCl / ethanol / Ambient temperature

7: 98 percent / dimethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / Ambient temperature

8: 54 percent / NaBH₄, 2 N H₂SO₄ / ethanol / 0 °C

9: 1.) Et₃N, MeSO₂Cl / 1.) THF, -30 deg C to room temperature, 15 min, 2.) 90 min

10: 69 percent / BF₃*Et₂O, CaH₂ / CH₂Cl₂ / 60 h

11: 1.) ozone, 2.) dimethyl sulfide / 1.) CH₂Cl₂, - 78 deg C, 2.) -78 deg C to room temperature, 2 h

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; calcium hydride; dimethylsulfide; sulfuric acid; boron trifluoride diethyl etherate; hydrogen; ozone; methanesulfonyl chloride; dimethyl azodicarboxylate; triethylamine; triphenylphosphine; dmap; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; toluene; tert-butyl alcohol;
DOI:10.1016/S0040-4020(01)90540-X

Reference yield:

: 132143-08-9
1-(tert-Butyl-dimethyl-silanyl)-3-(2-nitro-phenyl)-pyrrolidine-2,5-dione

: 132143-02-3
C₂₇H₃₀N₂O₄

Guidance literature:: Multi-step reaction with 10 steps

1: 95 percent / H₂ / 10percent Pd/C / toluene; ethanol / 18 h / 760 Torr

2: toluene / Ambient temperature

3: 1.5 M n-BuLi / 2-methyl-propan-2-ol; tetrahydrofuran; hexane; toluene / 0.5 h / 5 °C

4: toluene

5: 20percent aq. HCl / ethanol / Ambient temperature

6: 98 percent / dimethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / Ambient temperature

7: 54 percent / NaBH₄, 2 N H₂SO₄ / ethanol / 0 °C

8: 1.) Et₃N, MeSO₂Cl / 1.) THF, -30 deg C to room temperature, 15 min, 2.) 90 min

9: 69 percent / BF₃*Et₂O, CaH₂ / CH₂Cl₂ / 60 h

10: 1.) ozone, 2.) dimethyl sulfide / 1.) CH₂Cl₂, - 78 deg C, 2.) -78 deg C to room temperature, 2 h

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; calcium hydride; dimethylsulfide; sulfuric acid; boron trifluoride diethyl etherate; hydrogen; ozone; methanesulfonyl chloride; dimethyl azodicarboxylate; triethylamine; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; toluene; tert-butyl alcohol;
DOI:10.1016/S0040-4020(01)90540-X

Reference yield:

: 772-01-0
2-phenyl-1,3-dioxane

: 132143-02-3
C₂₇H₃₀N₂O₄

Guidance literature:: Multi-step reaction with 11 steps

1: 93 percent / 1.5 M DIBAL-H / toluene / Ambient temperature

2: 82 percent / pyridine/CrO₃ complex / CH₂Cl₂

3: toluene / Ambient temperature

4: 1.5 M n-BuLi / 2-methyl-propan-2-ol; tetrahydrofuran; hexane; toluene / 0.5 h / 5 °C

5: toluene

6: 20percent aq. HCl / ethanol / Ambient temperature

7: 98 percent / dimethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran / Ambient temperature

8: 54 percent / NaBH₄, 2 N H₂SO₄ / ethanol / 0 °C

9: 1.) Et₃N, MeSO₂Cl / 1.) THF, -30 deg C to room temperature, 15 min, 2.) 90 min

10: 69 percent / BF₃*Et₂O, CaH₂ / CH₂Cl₂ / 60 h

11: 1.) ozone, 2.) dimethyl sulfide / 1.) CH₂Cl₂, - 78 deg C, 2.) -78 deg C to room temperature, 2 h

With pyridine; chromium(VI) oxide; hydrogenchloride; sodium tetrahydroborate; n-butyllithium; calcium hydride; dimethylsulfide; sulfuric acid; boron trifluoride diethyl etherate; diisobutylaluminium hydride; ozone; methanesulfonyl chloride; dimethyl azodicarboxylate; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; hexane; dichloromethane; toluene; tert-butyl alcohol;
DOI:10.1016/S0040-4020(01)90540-X