Technology Process of C63H70O18
There total 5 articles about C63H70O18 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve;
In
dichloromethane;
at 20 ℃;
for 2h;
DOI:10.1055/s-2003-42109
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 89 percent / TMSOTf / CH2Cl2 / 3 h / 20 °C
2: HCl / methanol / 20 °C
3: 86 percent / TMSOTf; 4 Angstroem molecular sieves / CH2Cl2 / 2 h / 20 °C
With
hydrogenchloride; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve;
In
methanol; dichloromethane;
DOI:10.1055/s-2003-42109
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 85 percent / PhCH2NH2 / tetrahydrofuran / 24 h / 20 °C
2: 84 percent / DBU / CH2Cl2 / 5 h / 20 °C
3: 89 percent / TMSOTf / CH2Cl2 / 3 h / 20 °C
4: HCl / methanol / 20 °C
5: 86 percent / TMSOTf; 4 Angstroem molecular sieves / CH2Cl2 / 2 h / 20 °C
With
hydrogenchloride; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; 1,8-diazabicyclo[5.4.0]undec-7-ene; benzylamine;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1055/s-2003-42109