{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}acetonitrile

Base Information

Chemical Name:{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}acetonitrile
CAS No.:1356600-74-2
Molecular Formula:C₂₄H₂₂N₂O₃
Molecular Weight:386.45
Hs Code.:

Synonyms:{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}acetonitrile

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Chemical Property of {4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}acetonitrile

Chemical Property:

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Technology Process of {4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}acetonitrile

There total 2 articles about {4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142533-52-6
(Z)-2-bromo-1-phenylethanone O-methyl oxime

: 1356600-74-2
{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}acetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 0.08 h / 20 °C

1.2: 5 h / 20 - 80 °C

2.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 16 h / 0 - 20 °C

With tributylphosphine; potassium carbonate; 1,1'-azodicarbonyl-dipiperidine; In toluene; acetonitrile;

Reference yield:

: 31376-92-8
(1E,1Z)-2-bromo-N-methoxy-1-phenylethanimine

: 1356600-74-2
{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}acetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 2 h / 82 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 12 h / 0 - 20 °C

With di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetonitrile;

Reference yield:

: 1356600-74-2
{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}acetonitrile

: 105-36-2
ethyl bromoacetate

: 1356603-00-3
ethyl 3-cyano-3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Guidance literature:: {4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}acetonitrile; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

ethyl bromoacetate; In N,N-dimethyl-formamide; at 10 ℃; for 4h;