1,1-dimethylethyl (2R)-2-({[4-(hydrazinocarbonyl)phenyl]oxy}methyl)-4-morpholinecarboxylate

Base Information

Chemical Name:1,1-dimethylethyl (2R)-2-({[4-(hydrazinocarbonyl)phenyl]oxy}methyl)-4-morpholinecarboxylate
CAS No.:1093988-39-6
Molecular Formula:C₁₇H₂₅N₃O₅
Molecular Weight:351.403
Hs Code.:

Synonyms:1,1-dimethylethyl (2R)-2-({[4-(hydrazinocarbonyl)phenyl]oxy}methyl)-4-morpholinecarboxylate

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Chemical Property of 1,1-dimethylethyl (2R)-2-({[4-(hydrazinocarbonyl)phenyl]oxy}methyl)-4-morpholinecarboxylate

Chemical Property:

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Technology Process of 1,1-dimethylethyl (2R)-2-({[4-(hydrazinocarbonyl)phenyl]oxy}methyl)-4-morpholinecarboxylate

There total 7 articles about 1,1-dimethylethyl (2R)-2-({[4-(hydrazinocarbonyl)phenyl]oxy}methyl)-4-morpholinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1093988-38-5
1,1-dimethylethyl (2R)-2-[({4-[(methyloxy)carbonyl]phenyl}oxy)methyl]-4-morpholinecarboxylate

: 1093988-39-6
1,1-dimethylethyl (2R)-2-({[4-(hydrazinocarbonyl)phenyl]oxy}methyl)-4-morpholinecarboxylate

Guidance literature:: With hydrazine; In ethanol; for 4h; Reflux;

Reference yield:

: 929278-88-6
N-(2-hydroxyethyl)-N-{(2R)-2-hydroxy-3-[(phenylmethyl)oxy]propyl}-4-methylbenzenesulfonamide

: 1093988-39-6
1,1-dimethylethyl (2R)-2-({[4-(hydrazinocarbonyl)phenyl]oxy}methyl)-4-morpholinecarboxylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran; hexane; mineral oil / 1 h / 0 - 20 °C

1.2: 20 °C

1.3: 0 °C

2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 144 h / 760.05 Torr

3.1: naphthalene; sodium / tetrahydrofuran / 0.08 h / 0 °C

4.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 0.42 h / 120 °C / microwave reactor

6.1: hydrazine / ethanol / 4 h / Reflux

With dmap; naphthalene; hydrogen; sodium; sodium hydride; potassium carbonate; triethylamine; hydrazine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; hexane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 929278-86-4
(2R)-1-[(2-hydroxyethyl)amino]-3-[(phenylmethyl)oxy]-2-propanol

: 1093988-39-6
1,1-dimethylethyl (2R)-2-({[4-(hydrazinocarbonyl)phenyl]oxy}methyl)-4-morpholinecarboxylate

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / dichloromethane / 5 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; hexane; mineral oil / 1 h / 0 - 20 °C

2.2: 20 °C

2.3: 0 °C

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 144 h / 760.05 Torr

4.1: naphthalene; sodium / tetrahydrofuran / 0.08 h / 0 °C

5.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

6.1: potassium carbonate / N,N-dimethyl-formamide / 0.42 h / 120 °C / microwave reactor

7.1: hydrazine / ethanol / 4 h / Reflux

With dmap; naphthalene; hydrogen; sodium; sodium hydride; potassium carbonate; triethylamine; hydrazine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; hexane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;