methanesulfonic acid trans-(3S,6R)-6-benzhydryl-tetrahydropyran-3-yl ester

Base Information

Chemical Name:methanesulfonic acid trans-(3S,6R)-6-benzhydryl-tetrahydropyran-3-yl ester
CAS No.:869114-37-4
Molecular Formula:C₁₉H₂₂O₄S
Molecular Weight:346.447
Hs Code.:

Synonyms:methanesulfonic acid trans-(3S,6R)-6-benzhydryl-tetrahydropyran-3-yl ester

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Chemical Property of methanesulfonic acid trans-(3S,6R)-6-benzhydryl-tetrahydropyran-3-yl ester

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Technology Process of methanesulfonic acid trans-(3S,6R)-6-benzhydryl-tetrahydropyran-3-yl ester

There total 2 articles about methanesulfonic acid trans-(3S,6R)-6-benzhydryl-tetrahydropyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 869114-37-4
methanesulfonic acid trans-(3S,6R)-6-benzhydryl-tetrahydropyran-3-yl ester

Guidance literature:

Reference yield:

: 862647-20-9
(1R,4R,6S)-4-benzhydryl-3,7-dioxabicyclo[4.1.0]heptane

: 124-63-0
methanesulfonyl chloride

: 869114-37-4
methanesulfonic acid trans-(3S,6R)-6-benzhydryl-tetrahydropyran-3-yl ester

: Methanesulfonic acid (2R,4R)-2-benzhydryl-tetrahydro-pyran-4-yl ester

Guidance literature:: (1R,4R,6S)-4-benzhydryl-3,7-dioxabicyclo[4.1.0]heptane; With lithium aluminium tetrahydride; In diethyl ether; hexane; at 20 ℃; for 20h;

methanesulfonyl chloride; With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/jm0601699

Reference yield:

: 869114-37-4
methanesulfonic acid trans-(3S,6R)-6-benzhydryl-tetrahydropyran-3-yl ester

: 869114-40-9
cis-(3R,6R)-(6-benzhydryl-tetrahydropyran-3-yl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaN₃ / dimethylformamide / 100 °C

2: 92 percent / H₂ / Pd/C / methanol / 4 h

With sodium azide; hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm0601699