2-(3,4-dimethoxyphenyl)-1-(3-(4-(methylamino)phenyl)-4,5-dihydro-1H-pyrazol-1-yl)ethanone

Base Information

Chemical Name:2-(3,4-dimethoxyphenyl)-1-(3-(4-(methylamino)phenyl)-4,5-dihydro-1H-pyrazol-1-yl)ethanone
CAS No.:1076690-13-5
Molecular Formula:C₂₀H₂₃N₃O₃
Molecular Weight:353.421
Hs Code.:

Synonyms:2-(3,4-dimethoxyphenyl)-1-(3-(4-(methylamino)phenyl)-4,5-dihydro-1H-pyrazol-1-yl)ethanone

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Chemical Property of 2-(3,4-dimethoxyphenyl)-1-(3-(4-(methylamino)phenyl)-4,5-dihydro-1H-pyrazol-1-yl)ethanone

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Technology Process of 2-(3,4-dimethoxyphenyl)-1-(3-(4-(methylamino)phenyl)-4,5-dihydro-1H-pyrazol-1-yl)ethanone

There total 2 articles about 2-(3,4-dimethoxyphenyl)-1-(3-(4-(methylamino)phenyl)-4,5-dihydro-1H-pyrazol-1-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 1076690-12-4
1-[3-(4-amino-phenyl)-4,5-dihydro-pyrazol-1-yl]-2-(3,4-dimethoxy-phenyl)-ethanone

: 74-88-4
methyl iodide

: 1076690-13-5
2-(3,4-dimethoxyphenyl)-1-(3-(4-(methylamino)phenyl)-4,5-dihydro-1H-pyrazol-1-yl)ethanone

: C₂₁H₂₅N₃O₃

Guidance literature:: In N,N-dimethyl-formamide; acetonitrile; at 60 ℃; for 0.5h;

Reference yield:

: 1076690-77-1
2-(3,4-dimethoxy-phenyl)-1-[3-(4-nitro-phenyl)-4,5-dihydro-pyrazol-1-yl]-ethanone

: 1076690-13-5
2-(3,4-dimethoxyphenyl)-1-(3-(4-(methylamino)phenyl)-4,5-dihydro-1H-pyrazol-1-yl)ethanone

: C₂₁H₂₅N₃O₃

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / acetonitrile / 5 h

2: N,N-dimethyl-formamide; acetonitrile / 0.5 h / 60 °C

With hydrogen; palladium 10% on activated carbon; In N,N-dimethyl-formamide; acetonitrile;