4'-monomethoxytrityl 2,3,4-tri-O-benzyl-1-thio-1-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:4'-monomethoxytrityl 2,3,4-tri-O-benzyl-1-thio-1-deoxy-α-D-glucopyranoside
CAS No.:1393083-69-6
Molecular Formula:C₄₇H₄₆O₆S
Molecular Weight:738.945
Hs Code.:

Synonyms:4'-monomethoxytrityl 2,3,4-tri-O-benzyl-1-thio-1-deoxy-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4'-monomethoxytrityl 2,3,4-tri-O-benzyl-1-thio-1-deoxy-α-D-glucopyranoside

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Technology Process of 4'-monomethoxytrityl 2,3,4-tri-O-benzyl-1-thio-1-deoxy-α-D-glucopyranoside

There total 1 articles about 4'-monomethoxytrityl 2,3,4-tri-O-benzyl-1-thio-1-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 10548-46-6
1,6-anhydro-2,3,4-tri-O-benzyl-β-D-glucopyranose

: 383401-03-4
4-monomethoxytriphenylmethanethiol

: 1393083-69-6
4'-monomethoxytrityl 2,3,4-tri-O-benzyl-1-thio-1-deoxy-α-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 - 40 ℃; for 24h;
DOI:10.1016/j.tetlet.2012.05.159

Reference yield: 97.0%

: 1393083-69-6
4'-monomethoxytrityl 2,3,4-tri-O-benzyl-1-thio-1-deoxy-α-D-glucopyranoside

: 108-24-7
acetic anhydride

: 1393083-70-9
4'-monomethoxytrityl 6-O-acetyl-2,3,4-tri-O-benzyl-1-thio-1-deoxy-α-D-glucopyranoside

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1016/j.tetlet.2012.05.159

Reference yield:

: 1393083-69-6
4'-monomethoxytrityl 2,3,4-tri-O-benzyl-1-thio-1-deoxy-α-D-glucopyranoside

: 1393083-67-4
6-O-acetyl-2,3,4,2′,3′,4′,6′-hepta-O-benzyl-1-thio-α,α-D-trehalose

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 20 °C

2: triethylsilane; trifluoroacetic acid / dichloromethane

3: trimethylsilyl trifluoromethanesulfonate / diethyl ether; dichloromethane / 0.5 h / -78 °C / Inert atmosphere

With pyridine; triethylsilane; trimethylsilyl trifluoromethanesulfonate; trifluoroacetic acid; In diethyl ether; dichloromethane;
DOI:10.1016/j.tetlet.2012.05.159