((E)-6-Benzyloxy-4-methyl-hex-4-enylidene)-triphenyl-λ⁵-phosphane

Base Information Edit

Chemical Name:((E)-6-Benzyloxy-4-methyl-hex-4-enylidene)-triphenyl-λ⁵-phosphane
CAS No.:121926-70-3
Molecular Formula:C₃₂H₃₃OP
Molecular Weight:464.587
Hs Code.:
Mol file:121926-70-3.mol

((E)-6-Benzyloxy-4-methyl-hex-4-enylidene)-triphenyl-λ<sup>5</sup>-phosphane

Synonyms:((E)-6-Benzyloxy-4-methyl-hex-4-enylidene)-triphenyl-λ⁵-phosphane

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Chemical Property of ((E)-6-Benzyloxy-4-methyl-hex-4-enylidene)-triphenyl-λ⁵-phosphane Edit

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Technology Process of ((E)-6-Benzyloxy-4-methyl-hex-4-enylidene)-triphenyl-λ⁵-phosphane

There total 6 articles about ((E)-6-Benzyloxy-4-methyl-hex-4-enylidene)-triphenyl-λ⁵-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121926-73-6
(E)-(6-benzyloxy-4-methyl-4-hexenyl)triphenylphosphonium iodide

: 121926-70-3
((E)-6-Benzyloxy-4-methyl-hex-4-enylidene)-triphenyl-λ⁵-phosphane

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; In hexane; at -65 ℃; for 3.5h;
DOI:10.1246/bcsj.63.1629

Reference yield:

: 52188-73-5
geranyl benzyl ether

: 121926-70-3
((E)-6-Benzyloxy-4-methyl-hex-4-enylidene)-triphenyl-λ⁵-phosphane

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) N-bromosuccinimide 2.) KOH

2: periodic acid

3: sodium borohydride

5: butyllithium / tetrahydrofuran; hexamethylphosphoric acid triamide

With potassium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; n-butyllithium; periodic acid; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1246/cl.1988.1433

Reference yield:

: 98066-00-3
(E)-4-methyl-6-(phenylmethoxy)-4-hexen-1-ol

: 121926-70-3
((E)-6-Benzyloxy-4-methyl-hex-4-enylidene)-triphenyl-λ⁵-phosphane

Guidance literature:: Multi-step reaction with 2 steps

2: butyllithium / tetrahydrofuran; hexamethylphosphoric acid triamide

With n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1246/cl.1988.1433