2,3-dehydrodeoxamuscarone

Base Information

Chemical Name:2,3-dehydrodeoxamuscarone
CAS No.:79195-22-5
Molecular Formula:C₁₀H₁₈NO*I
Molecular Weight:295.164
Hs Code.:

Synonyms:2-Cyclopentene-1-methanaminium,N,N,N,3-tetramethyl-4-oxo-, iodide (9CI)

Suppliers and Price of 2,3-dehydrodeoxamuscarone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 2,3-dehydrodeoxamuscarone

Chemical Property:

PSA：32.29000
LogP:-0.78890

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3-dehydrodeoxamuscarone

There total 10 articles about 2,3-dehydrodeoxamuscarone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 3-methyl-4-oxo-1-(N,N-dimethylaminomethyl)cyclopent-2-ene

: 74-88-4
methyl iodide

: 79195-22-5
2,3-dehydrodeoxamuscarone

Guidance literature:: In diethyl ether; Ambient temperature;
DOI:10.1002/jps.2600700506

Reference yield:

: 3-methyl-4-oxo-1-carbomethoxycyclopent-2-ene

: 79195-22-5
2,3-dehydrodeoxamuscarone

Guidance literature:: Multi-step reaction with 5 steps

1: 0.42 g / 9-borabicyclo<3.3.1>nonane / tetrahydrofuran / 1) 0 deg C, 4 h; 2) 25 deg C, 2 h

2: 0.25 g / 48 h / 95 - 100 °C

3: 0.26 g / LiAlH₄ / tetrahydrofuran / 5 h / Heating

4: 1.0 g / chromium trioxide, aq. H₂SO₄ / 2 h / Ambient temperature

5: 80 percent / diethyl ether / Ambient temperature

With chromium(VI) oxide; lithium aluminium tetrahydride; 9-borabicyclo[3.3.1]nonane dimer; sulfuric acid; In tetrahydrofuran; diethyl ether;
DOI:10.1002/jps.2600700506

Reference yield:

: (S)-3-Methyl-4-oxo-cyclopentanecarboxylic acid methyl ester

: 79195-22-5
2,3-dehydrodeoxamuscarone

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) Br₂ / 1) CCl₄, 0 deg C; 2) 120 deg C, 15 min, 50 mm pressure

2: 0.42 g / 9-borabicyclo<3.3.1>nonane / tetrahydrofuran / 1) 0 deg C, 4 h; 2) 25 deg C, 2 h

3: 0.25 g / 48 h / 95 - 100 °C

4: 0.26 g / LiAlH₄ / tetrahydrofuran / 5 h / Heating

5: 1.0 g / chromium trioxide, aq. H₂SO₄ / 2 h / Ambient temperature

6: 80 percent / diethyl ether / Ambient temperature

With chromium(VI) oxide; lithium aluminium tetrahydride; 9-borabicyclo[3.3.1]nonane dimer; sulfuric acid; bromine; In tetrahydrofuran; diethyl ether;
DOI:10.1002/jps.2600700506