methyl 3-(4-[4-[1-(2-chlorophenyl)ethoxycarbonylamino]-5-isoxazolyl]benzylsulfanyl)propionate

Base Information

Chemical Name:methyl 3-(4-[4-[1-(2-chlorophenyl)ethoxycarbonylamino]-5-isoxazolyl]benzylsulfanyl)propionate
CAS No.:946149-64-0
Molecular Formula:C₂₃H₂₃ClN₂O₅S
Molecular Weight:474.965
Hs Code.:

Synonyms:methyl 3-(4-[4-[1-(2-chlorophenyl)ethoxycarbonylamino]-5-isoxazolyl]benzylsulfanyl)propionate

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Chemical Property of methyl 3-(4-[4-[1-(2-chlorophenyl)ethoxycarbonylamino]-5-isoxazolyl]benzylsulfanyl)propionate

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Technology Process of methyl 3-(4-[4-[1-(2-chlorophenyl)ethoxycarbonylamino]-5-isoxazolyl]benzylsulfanyl)propionate

There total 11 articles about methyl 3-(4-[4-[1-(2-chlorophenyl)ethoxycarbonylamino]-5-isoxazolyl]benzylsulfanyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 839718-31-9
5-(4-{[(3-methoxy-3-oxopropyl)thio]methyl}phenyl)isoxazole-4-carboxylic acid

: 13524-04-4
2'-chloro-sec-phenethyl alcohol

: 946149-64-0
methyl 3-(4-[4-[1-(2-chlorophenyl)ethoxycarbonylamino]-5-isoxazolyl]benzylsulfanyl)propionate

Guidance literature:: With diphenyl-phosphinic acid; triethylamine; In toluene; at 90 ℃; for 0.666667h;
DOI:10.1016/j.bmcl.2007.04.024

Reference yield: 20.0%

: 946149-64-0
methyl 3-(4-[4-[1-(2-chlorophenyl)ethoxycarbonylamino]-5-isoxazolyl]benzylsulfanyl)propionate

Guidance literature:

Reference yield:

: C₁₉H₂₄O₆S

: 946149-64-0
methyl 3-(4-[4-[1-(2-chlorophenyl)ethoxycarbonylamino]-5-isoxazolyl]benzylsulfanyl)propionate

Guidance literature:: Multi-step reaction with 3 steps

1: NH₂OH / ethanol / 2 h / 70 °C

2: 98 percent / HCl / dioxane / 21 h / 100 °C

3: 20 percent / DPPA; NEt₃ / toluene / 0.67 h / 90 °C

With hydrogenchloride; diphenyl-phosphinic acid; hydroxylamine; triethylamine; In 1,4-dioxane; ethanol; toluene;
DOI:10.1016/j.bmcl.2007.04.024