methyl <4--3-(tert-butoxycarbonyl)propoxy>benzoyl>formate

Base Information

Chemical Name:methyl <4--3-(tert-butoxycarbonyl)propoxy>benzoyl>formate
CAS No.:110207-50-6
Molecular Formula:C₂₂H₃₁NO₈
Molecular Weight:437.49
Hs Code.:

methyl <4-<D-3-<(tert-butoxycarbonyl)amino>-3-(tert-butoxycarbonyl)propoxy>benzoyl>formate

Synonyms:methyl <4--3-(tert-butoxycarbonyl)propoxy>benzoyl>formate

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Chemical Property of methyl <4--3-(tert-butoxycarbonyl)propoxy>benzoyl>formate

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Technology Process of methyl <4--3-(tert-butoxycarbonyl)propoxy>benzoyl>formate

There total 3 articles about methyl <4--3-(tert-butoxycarbonyl)propoxy>benzoyl>formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 38250-16-7
4-hydroxy-alpha-oxobenzeneacetic acid methyl ester

: 110207-49-3
tert-butyl D-N-(tert-butoxycarbonyl)homoserinate

: 110207-50-6
methyl <4--3-(tert-butoxycarbonyl)propoxy>benzoyl>formate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; Ambient temperature;
DOI:10.1016/S0040-4039(00)83888-5

Reference yield:

: 77004-75-2
(3R)-4-tert-butoxy-3-[(tert-butoxycarbonyl)amino]-4-oxobutanoic acid

: 110207-50-6
methyl <4--3-(tert-butoxycarbonyl)propoxy>benzoyl>formate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) triethylamine, ethyl chloroformate, 2.) sodium borohydride / 1.) THF, RT, 30 min, 2.) water, RT, 4 h

2: 74 percent / triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 0.5 h

With sodium tetrahydroborate; chloroformic acid ethyl ester; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1021/ja00158a040

Reference yield:

: 54537-30-3
p-hydroxybenzoylformic acid sodium salt

: 110207-50-6
methyl <4--3-(tert-butoxycarbonyl)propoxy>benzoyl>formate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / dimethylsulfoxide / 18 h

2: 74 percent / triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 0.5 h

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/ja00158a040