C₃₃H₃₄O₄S

Base Information

Chemical Name:C₃₃H₃₄O₄S
CAS No.:1002099-21-9
Molecular Formula:C₃₃H₃₄O₄S
Molecular Weight:526.697
Hs Code.:

C<sub>33</sub>H<sub>34</sub>O<sub>4</sub>S

Synonyms:C₃₃H₃₄O₄S

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Chemical Property of C₃₃H₃₄O₄S

Chemical Property:

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Technology Process of C₃₃H₃₄O₄S

There total 4 articles about C₃₃H₃₄O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₂O₄S

: 100-39-0
benzyl bromide

: 1002099-21-9
C₃₃H₃₄O₄S

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo102382r

Reference yield:

: 1279711-37-3
C₂₇H₂₈O₆S

: 1002099-21-9
C₃₃H₃₄O₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.75 h / 0 - 20 °C

1.2: 16 h / 20 °C

2.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 0.5 h / Reflux

3.1: acetic acid / tetrahydrofuran; water / 5 h / 45 °C

4.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide; mineral oil / 20 °C / Inert atmosphere

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; acetic acid; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/jo102382r

Reference yield:

: 1315305-92-0
C₂₉H₃₀O₆S₃

: 1002099-21-9
C₃₃H₃₄O₄S

Guidance literature:: Multi-step reaction with 3 steps

1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 0.5 h / Reflux

2: acetic acid / tetrahydrofuran; water / 5 h / 45 °C

3: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide; mineral oil / 20 °C / Inert atmosphere

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; acetic acid; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/jo102382r