1-((cyclopentylidene(isocyano)methyl)sulfonyl)-4-methylbenzene

Base Information

• Chemical Name: 1-((cyclopentylidene(isocyano)methyl)sulfonyl)-4-methylbenzene
• CAS No.: 74153-35-8
• Molecular Formula: C₁₄H₁₅NO₂S
• Molecular Weight: 261.345
• Mol file: 74153-35-8.mol

Synonyms:1-((cyclopentylidene(isocyano)methyl)sulfonyl)-4-methylbenzene

Chemical Property of 1-((cyclopentylidene(isocyano)methyl)sulfonyl)-4-methylbenzene

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1-((cyclopentylidene(isocyano)methyl)sulfonyl)-4-methylbenzene

There total 1 articles about 1-((cyclopentylidene(isocyano)methyl)sulfonyl)-4-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[(p-methylphenyl)sulfonylmethyl]isonitrile (38622-91-2,36635-61-7) + cyclopentanone (120-92-3) → 1-((cyclopentylidene(isocyano)methyl)sulfonyl)-4-methylbenzene (74153-35-8)

Guidance literature:

DOI:10.1016/S0040-4039(01)81237-5

Reference yield: 79.0%

1-((cyclopentylidene(isocyano)methyl)sulfonyl)-4-methylbenzene (74153-35-8) + methyl iodide (74-88-4) → C15H17NO2S (91890-27-6)

Guidance literature:

With potassium tert-butylate; In 1,2-dimethoxyethane; 1) -30 deg C, 2) -30 to 20 deg C, 1 h;

DOI:10.1016/S0040-4039(01)81237-5

Reference yield: 70.0%

cinnamaldehyde N-(4-nitrophenyl)imine (15286-45-0,56110-09-9) + 1-((cyclopentylidene(isocyano)methyl)sulfonyl)-4-methylbenzene (74153-35-8) → 4-Cyclopent-1-enyl-1-(4-nitro-phenyl)-5-((E)-styryl)-1H-imidazole (106724-45-2)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; -78 deg C to 20 deg C in 2 h;

DOI:10.1016/S0040-4039(00)84479-2

upstream raw materials:

[(p-methylphenyl)sulfonylmethyl]isonitrile

cyclopentanone

Downstream raw materials:

C₁₇H₂₁NO₂S

4-Cyclopent-1-enyl-1-(4-nitro-phenyl)-5-((E)-styryl)-1H-imidazole

C₁₆H₁₈BrNO₂S

C₃₁H₃₄N₂O₄S₂