C₄₄H₄₀N₄O₁₂S₂

Base Information

Chemical Name:C₄₄H₄₀N₄O₁₂S₂
CAS No.:1262795-79-8
Molecular Formula:C₄₄H₄₀N₄O₁₂S₂
Molecular Weight:880.953
Hs Code.:

C<sub>44</sub>H<sub>40</sub>N<sub>4</sub>O<sub>12</sub>S<sub>2</sub>

Synonyms:C₄₄H₄₀N₄O₁₂S₂

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Chemical Property of C₄₄H₄₀N₄O₁₂S₂

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Technology Process of C₄₄H₄₀N₄O₁₂S₂

There total 7 articles about C₄₄H₄₀N₄O₁₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1262795-65-2
C₂₂H₂₀N₂O₆S

: C₂₂H₂₀N₂O₆S

: 1262795-79-8
C₄₄H₄₀N₄O₁₂S₂

Guidance literature:: With N,N'-bis(benzyliden)ethylendiamine; palladium(II) acetate; In 1,2-dichloro-ethane; at 56 ℃; for 4h; Inert atmosphere;
DOI:10.1071/CH10359

Reference yield:

: 161196-42-5
2-bromocyclohex-2-enylamine

: C₂₂H₂₀N₂O₆S

: 1262795-79-8
C₄₄H₄₀N₄O₁₂S₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; triethylamine / dichloromethane / 1.5 h / 18 °C / Inert atmosphere

2.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / tetrahydrofuran; water / 1.5 h / 90 °C / Microwave irradiation; Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

3.2: 3 h / 0 - 18 °C / Inert atmosphere

4.1: palladium(II) acetate; N,N'-bis(benzyliden)ethylendiamine / 1,2-dichloro-ethane / 4 h / 56 °C / Inert atmosphere

With dmap; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; N,N'-bis(benzyliden)ethylendiamine; palladium(II) acetate; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil; 2.1: Suzuki coupling;
DOI:10.1071/CH10359

Reference yield:

: 1262795-58-3
C₁₁H₁₈BrNO₂

: C₂₂H₂₀N₂O₆S

: 1262795-79-8
C₄₄H₄₀N₄O₁₂S₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluoroacetic acid / dichloromethane / 2.5 h / 18 °C / Inert atmosphere

2.1: dmap; triethylamine / dichloromethane / 1.5 h / 18 °C / Inert atmosphere

3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / tetrahydrofuran; water / 1.5 h / 90 °C / Microwave irradiation; Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

4.2: 3 h / 0 - 18 °C / Inert atmosphere

5.1: palladium(II) acetate; N,N'-bis(benzyliden)ethylendiamine / 1,2-dichloro-ethane / 4 h / 56 °C / Inert atmosphere

With dmap; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; N,N'-bis(benzyliden)ethylendiamine; palladium(II) acetate; sodium hydride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil; 3.1: Suzuki coupling;
DOI:10.1071/CH10359