C₃₉H₅₃N₃O₅

Base Information

Chemical Name:C₃₉H₅₃N₃O₅
CAS No.:743460-71-1
Molecular Formula:C₃₉H₅₃N₃O₅
Molecular Weight:643.867
Hs Code.:

C<sub>39</sub>H<sub>53</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₃₉H₅₃N₃O₅

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Chemical Property of C₃₉H₅₃N₃O₅

Chemical Property:

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Technology Process of C₃₉H₅₃N₃O₅

There total 9 articles about C₃₉H₅₃N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17337-13-2
[1,1'-biphenyl]-2-yl-isocyanate

: 743460-71-1
C₃₉H₅₃N₃O₅

Guidance literature:: Multi-step reaction with 8 steps

1: 70 °C / neat (no solvent)

2: 10% palladium on activated charcoal; ammonium bicarbonate / ethanol / 40 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 50 °C

4: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C

5: sodium tris(acetoxy)borohydride / methanol; dichloromethane

6: 20 % Pd(OH)2/C; hydrogen / ethanol

7: sodium hydrogencarbonate; sodium iodide / tetrahydrofuran / 80 °C

8: triethylamine tris(hydrogen fluoride) / dichloromethane; N,N-dimethyl-formamide

With 10% palladium on activated charcoal; 20 % Pd(OH)2/C; hydrogen; sulfur trioxide pyridine complex; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; ammonium bicarbonate; dimethyl sulfoxide; triethylamine tris(hydrogen fluoride); N-ethyl-N,N-diisopropylamine; sodium iodide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.01.043

Reference yield:

: 852291-44-2
biphenyl-2-ylcarbamic acid 1-(9-hydroxynonyl)piperidin-4-yl ester

: 743460-71-1
C₃₉H₅₃N₃O₅

Guidance literature:: Multi-step reaction with 5 steps

1: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C

2: sodium tris(acetoxy)borohydride / methanol; dichloromethane

3: 20 % Pd(OH)2/C; hydrogen / ethanol

4: sodium hydrogencarbonate; sodium iodide / tetrahydrofuran / 80 °C

5: triethylamine tris(hydrogen fluoride) / dichloromethane; N,N-dimethyl-formamide

With 20 % Pd(OH)2/C; hydrogen; sulfur trioxide pyridine complex; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; dimethyl sulfoxide; triethylamine tris(hydrogen fluoride); N-ethyl-N,N-diisopropylamine; sodium iodide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.01.043

Reference yield:

: 1289178-45-5
C₄₁H₅₁N₃O₂

: 743460-71-1
C₃₉H₅₃N₃O₅

Guidance literature:: Multi-step reaction with 3 steps

1: 20 % Pd(OH)2/C; hydrogen / ethanol

2: sodium hydrogencarbonate; sodium iodide / tetrahydrofuran / 80 °C

3: triethylamine tris(hydrogen fluoride) / dichloromethane; N,N-dimethyl-formamide

With 20 % Pd(OH)2/C; hydrogen; sodium hydrogencarbonate; triethylamine tris(hydrogen fluoride); sodium iodide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.01.043