N-benzyloxycarbonyl-1,4-dideoxy-1,4-imino-2,3-O-isopropylidene-D-allitol

Base Information

Chemical Name:N-benzyloxycarbonyl-1,4-dideoxy-1,4-imino-2,3-O-isopropylidene-D-allitol
CAS No.:405283-43-4
Molecular Formula:C₁₇H₂₃NO₆
Molecular Weight:337.373
Hs Code.:

Synonyms:N-benzyloxycarbonyl-1,4-dideoxy-1,4-imino-2,3-O-isopropylidene-D-allitol

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Chemical Property of N-benzyloxycarbonyl-1,4-dideoxy-1,4-imino-2,3-O-isopropylidene-D-allitol

Chemical Property:

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Technology Process of N-benzyloxycarbonyl-1,4-dideoxy-1,4-imino-2,3-O-isopropylidene-D-allitol

There total 4 articles about N-benzyloxycarbonyl-1,4-dideoxy-1,4-imino-2,3-O-isopropylidene-D-allitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 405283-44-5
N-(benzyloxycarbonyl)-1,4-dideoxy-1,4-imino-2,3:5,6-di-O-isopropylidene-D-allitol

: 405283-43-4
N-benzyloxycarbonyl-1,4-dideoxy-1,4-imino-2,3-O-isopropylidene-D-allitol

Guidance literature:: With water; acetic acid; at 20 ℃; for 10h;

Reference yield:

: 117859-46-8
1,4-Dideoxy-2,3:5,6-di-O-isopropylidene-1,4-imino-D-allitol

: 405283-43-4
N-benzyloxycarbonyl-1,4-dideoxy-1,4-imino-2,3-O-isopropylidene-D-allitol

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / NaHCO₃ / ethanol; H₂O / 2 h / 20 °C

2: 37 percent / H₂O; PTSA / methanol / 16 h / 20 °C

With water; sodium hydrogencarbonate; toluene-4-sulfonic acid; In methanol; ethanol; water;
DOI:10.1016/j.tetasy.2003.11.022

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 405283-43-4
N-benzyloxycarbonyl-1,4-dideoxy-1,4-imino-2,3-O-isopropylidene-D-allitol

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / NaHCO₃ / ethanol; H₂O / 0.67 h / 20 °C

2: 68 percent / AcOH; water / 10 h / 20 °C

With water; sodium hydrogencarbonate; acetic acid; In ethanol; water;