Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]chloromethylphosphonate

Base Information

Chemical Name:Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]chloromethylphosphonate
CAS No.:263165-14-6
Molecular Formula:C₂₀H₃₅ClO₆P₂
Molecular Weight:468.895
Hs Code.:

Synonyms:Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]chloromethylphosphonate

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Chemical Property of Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]chloromethylphosphonate

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Technology Process of Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]chloromethylphosphonate

There total 5 articles about Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]chloromethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 263165-10-2
Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]hydroxymethylphosphonate

: 263165-14-6
Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]chloromethylphosphonate

Guidance literature:: With thionyl chloride; In dichloromethane; for 12h; Heating;
DOI:10.1039/a906507e

Reference yield:

: 513-02-0
triisopropyl phosphate

: 263165-14-6
Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]chloromethylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / CH₂Cl₂ / 2 h / 20 °C

2: 50 percent / sodium borohydride / CH₂Cl₂; H₂O / 3 h / 20 °C

3: 61 percent / 36 h / 120 °C

4: 93 percent / thionyl chloride / CH₂Cl₂ / 12 h / Heating

With sodium tetrahydroborate; thionyl chloride; In dichloromethane; water; 1: Substitution / 2: Reduction / 3: Substitution / 4: Substitution;
DOI:10.1039/a906507e

Reference yield:

: 876-08-4
p-(chloromethyl)benzoyl chloride

: 263165-14-6
Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]chloromethylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / CH₂Cl₂ / 2 h / 20 °C

2: 50 percent / sodium borohydride / CH₂Cl₂; H₂O / 3 h / 20 °C

3: 61 percent / 36 h / 120 °C

4: 93 percent / thionyl chloride / CH₂Cl₂ / 12 h / Heating

With sodium tetrahydroborate; thionyl chloride; In dichloromethane; water; 1: Substitution / 2: Reduction / 3: Substitution / 4: Substitution;
DOI:10.1039/a906507e