Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]hydroxymethylphosphonate

Base Information

Chemical Name:Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]hydroxymethylphosphonate
CAS No.:263165-10-2
Molecular Formula:C₂₀H₃₆O₇P₂
Molecular Weight:450.449
Hs Code.:

Synonyms:Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]hydroxymethylphosphonate

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Chemical Property of Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]hydroxymethylphosphonate

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Technology Process of Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]hydroxymethylphosphonate

There total 4 articles about Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]hydroxymethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 513-02-0
triisopropyl phosphate

: 263165-08-8
Diisopropyl (4'-chloromethylphenyl)hydroxymethylphosphonate

: 263165-10-2
Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]hydroxymethylphosphonate

Guidance literature:: at 120 ℃; for 36h;
DOI:10.1039/a906507e

Reference yield:

: 513-02-0
triisopropyl phosphate

: 263165-10-2
Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]hydroxymethylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / CH₂Cl₂ / 2 h / 20 °C

2: 50 percent / sodium borohydride / CH₂Cl₂; H₂O / 3 h / 20 °C

3: 61 percent / 36 h / 120 °C

With sodium tetrahydroborate; In dichloromethane; water; 1: Substitution / 2: Reduction / 3: Substitution;
DOI:10.1039/a906507e

Reference yield:

: 876-08-4
p-(chloromethyl)benzoyl chloride

: 263165-10-2
Diisopropyl 4-[(diisopropoxyphosphoryl)methylphenyl]hydroxymethylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / CH₂Cl₂ / 2 h / 20 °C

2: 50 percent / sodium borohydride / CH₂Cl₂; H₂O / 3 h / 20 °C

3: 61 percent / 36 h / 120 °C

With sodium tetrahydroborate; In dichloromethane; water; 1: Substitution / 2: Reduction / 3: Substitution;
DOI:10.1039/a906507e