C₁₇H₁₉NO₄

Base Information

• Chemical Name: C₁₇H₁₉NO₄
• CAS No.: 156775-28-9
• Molecular Formula: C₁₇H₁₉NO₄
• Molecular Weight: 301.342
• Mol file: 156775-28-9.mol

Synonyms:C₁₇H₁₉NO₄

Chemical Property of C₁₇H₁₉NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₉NO₄

There total 4 articles about C₁₇H₁₉NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

C17H17NO4 → C17H19NO4 (156775-28-9)

Guidance literature:

With sodium tetrahydroborate; silica gel; In chloroform; isopropyl alcohol; at 25 ℃; for 0.25h;

DOI:10.1080/00397919408011304

Reference yield:

lysichitalexin (31236-71-2) → C17H19NO4 (156775-28-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / dimethylamine hydrochloride, KF / toluene / Heating

2: 70 percent / silica, NaBH₄ / propan-2-ol; CHCl₃ / 0.25 h / 25 °C

With potassium fluoride; sodium tetrahydroborate; N,N-dimethylammonium chloride; silica gel; In chloroform; isopropyl alcohol; toluene;

DOI:10.1080/00397919408011304

Reference yield:

(E)-1-methoxy-4-(2-nitrovinyl)benzene (3179-10-0,5576-97-6) → C17H19NO4 (156775-28-9)

Guidance literature:

Multi-step reaction with 3 steps

1: silica gel, NaBH₄ / CHCl₃; propan-2-ol / 0.25 h / 25 °C

2: 65 percent / dimethylamine hydrochloride, KF / toluene / Heating

3: 70 percent / silica, NaBH₄ / propan-2-ol; CHCl₃ / 0.25 h / 25 °C

With potassium fluoride; sodium tetrahydroborate; N,N-dimethylammonium chloride; silica gel; In chloroform; isopropyl alcohol; toluene;

DOI:10.1080/00397919408011304

upstream raw materials:

lysichitalexin

(E)-1-methoxy-4-(2-nitrovinyl)benzene

4-methoxy-benzaldehyde

Downstream raw materials:

1,3-bis(4-methoxyphenyl)acetone