3-{5,11-dioxo-5H,6H,11H-indeno[1,2-c]isoquinolin-6-yl}propyl 4-methylbenzene-1-sulfonate

Base Information

Chemical Name:3-{5,11-dioxo-5H,6H,11H-indeno[1,2-c]isoquinolin-6-yl}propyl 4-methylbenzene-1-sulfonate
CAS No.:1259520-40-5
Molecular Formula:C₂₆H₂₁NO₅S
Molecular Weight:459.522
Hs Code.:

Synonyms:3-{5,11-dioxo-5H,6H,11H-indeno[1,2-c]isoquinolin-6-yl}propyl 4-methylbenzene-1-sulfonate

Suppliers and Price of 3-{5,11-dioxo-5H,6H,11H-indeno[1,2-c]isoquinolin-6-yl}propyl 4-methylbenzene-1-sulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-{5,11-dioxo-5H,6H,11H-indeno[1,2-c]isoquinolin-6-yl}propyl 4-methylbenzene-1-sulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-{5,11-dioxo-5H,6H,11H-indeno[1,2-c]isoquinolin-6-yl}propyl 4-methylbenzene-1-sulfonate

There total 3 articles about 3-{5,11-dioxo-5H,6H,11H-indeno[1,2-c]isoquinolin-6-yl}propyl 4-methylbenzene-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 98-59-9
p-toluenesulfonyl chloride

: 6-(3-hydroxypropyl)-5H-indeno[1,2-c]isoquinoline-5,11(6H)-dione

: 1259520-40-5
3-{5,11-dioxo-5H,6H,11H-indeno[1,2-c]isoquinolin-6-yl}propyl 4-methylbenzene-1-sulfonate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1021/jm300335n

Reference yield:

: 5651-60-5
6-Oxa-benzo[a]fluorene-5,11-dione

: 1259520-40-5
3-{5,11-dioxo-5H,6H,11H-indeno[1,2-c]isoquinolin-6-yl}propyl 4-methylbenzene-1-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: chloroform / Reflux

2: dmap; triethylamine / dichloromethane / 16 h / 20 °C

With dmap; triethylamine; In dichloromethane; chloroform;
DOI:10.1021/jm300335n

Reference yield:

: 19147-02-5
2-(2-carboxyphenyl)indan-1,3-dione

: 1259520-40-5
3-{5,11-dioxo-5H,6H,11H-indeno[1,2-c]isoquinolin-6-yl}propyl 4-methylbenzene-1-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: water; toluene-4-sulfonic acid / benzene / 7 h / Reflux

2: chloroform / Reflux

3: dmap; triethylamine / dichloromethane / 16 h / 20 °C

With dmap; water; toluene-4-sulfonic acid; triethylamine; In dichloromethane; chloroform; benzene;
DOI:10.1021/jm300335n