C₁₆H₁₀Cl₂O₄

Base Information

Chemical Name:C₁₆H₁₀Cl₂O₄
CAS No.:1312609-89-4
Molecular Formula:C₁₆H₁₀Cl₂O₄
Molecular Weight:337.159
Hs Code.:

C<sub>16</sub>H<sub>10</sub>Cl<sub>2</sub>O<sub>4</sub>

Synonyms:C₁₆H₁₀Cl₂O₄

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Chemical Property of C₁₆H₁₀Cl₂O₄

Chemical Property:

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Technology Process of C₁₆H₁₀Cl₂O₄

There total 11 articles about C₁₆H₁₀Cl₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1312609-87-2
C₁₆H₁₂O₆

: 1312609-89-4
C₁₆H₁₀Cl₂O₄

Guidance literature:: With thionyl chloride; for 2h; Reflux;

Reference yield:

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 1312609-89-4
C₁₆H₁₀Cl₂O₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: pyridine / 24 h / 20 °C

2.1: nitric acid; sulfuric acid / 0.08 h / -40 °C

3.1: sodium hydroxide / water / 0.08 h

3.2: 85 °C

3.3: pH 2

4.1: water; hydrogen bromide; acetic acid / 4 h / Reflux

5.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 2068.65 Torr

6.1: sodium nitrite; hydrogen bromide / water / 2 h / 0 °C

6.2: 0 - 20 °C

7.1: sulfuric acid / 16 h / Reflux

8.1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

8.2: 12 h / 70 °C

9.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 10 h / 80 °C / Inert atmosphere

10.1: water; lithium hydroxide / tetrahydrofuran / 17 h / 20 °C

10.2: pH 2

11.1: thionyl chloride / 2 h / Reflux

With pyridine; thionyl chloride; sulfuric acid; water; hydrogen bromide; hydrogen; nitric acid; sodium carbonate; caesium carbonate; acetic acid; sodium hydroxide; lithium hydroxide; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; toluene; 9.1: Suzuki Coupling;

Reference yield:

: 7150-01-8
2-acetoxy-3-methoxybenzaldehyde

: 1312609-89-4
C₁₆H₁₀Cl₂O₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: nitric acid; sulfuric acid / 0.08 h / -40 °C

2.1: sodium hydroxide / water / 0.08 h

2.2: 85 °C

2.3: pH 2

3.1: water; hydrogen bromide; acetic acid / 4 h / Reflux

4.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 2068.65 Torr

5.1: sodium nitrite; hydrogen bromide / water / 2 h / 0 °C

5.2: 0 - 20 °C

6.1: sulfuric acid / 16 h / Reflux

7.1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

7.2: 12 h / 70 °C

8.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 10 h / 80 °C / Inert atmosphere

9.1: water; lithium hydroxide / tetrahydrofuran / 17 h / 20 °C

9.2: pH 2

10.1: thionyl chloride / 2 h / Reflux

With thionyl chloride; sulfuric acid; water; hydrogen bromide; hydrogen; nitric acid; sodium carbonate; caesium carbonate; acetic acid; sodium hydroxide; lithium hydroxide; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; toluene; 8.1: Suzuki Coupling;