2-tert-butyl-4-hydroxymethyl-5-(4-tert-butylbenzyl)mercapto-3-(2H)-pyridazinone

Base Information

• Chemical Name: 2-tert-butyl-4-hydroxymethyl-5-(4-tert-butylbenzyl)mercapto-3-(2H)-pyridazinone
• CAS No.: 1027097-05-7
• Molecular Formula: C₂₀H₂₈N₂O₂S
• Molecular Weight: 360.521

Synonyms:2-tert-butyl-4-hydroxymethyl-5-(4-tert-butylbenzyl)mercapto-3-(2H)-pyridazinone

Chemical Property of 2-tert-butyl-4-hydroxymethyl-5-(4-tert-butylbenzyl)mercapto-3-(2H)-pyridazinone

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2-tert-butyl-4-hydroxymethyl-5-(4-tert-butylbenzyl)mercapto-3-(2H)-pyridazinone

There total 1 articles about 2-tert-butyl-4-hydroxymethyl-5-(4-tert-butylbenzyl)mercapto-3-(2H)-pyridazinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-tert-butyl-4-(tert-butyldimethylsilyloxy)methyl-5-(4-tert-butylbenzyl)mercapto-3-(2H)-pyridazinone (1027097-04-6) → 2-tert-butyl-4-hydroxymethyl-5-(4-tert-butylbenzyl)mercapto-3-(2H)-pyridazinone (1027097-05-7)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 3h;

DOI:10.1021/jm701443n

Reference yield:

2-tert-butyl-4-hydroxymethyl-5-(4-tert-butylbenzyl)mercapto-3-(2H)-pyridazinone (1027097-05-7) + methanesulfonyl chloride (124-63-0) → 2-tert-butyl-4-(methanesulfonyloxy)methyl-5-(4-tert-butylbenzyl)mercapto-3-(2H)-pyridazinone (1027097-06-8)

Guidance literature:

With N,N,N'N'-tetramethyl-1,3-propanediamine; In acetonitrile; at 0 ℃; for 0.0833333h;

DOI:10.1021/jm701443n

Reference yield:

2-tert-butyl-4-hydroxymethyl-5-(4-tert-butylbenzyl)mercapto-3-(2H)-pyridazinone (1027097-05-7) + p-toluenesulfonyl chloride (98-59-9) → 2-tert-butyl-4-p-toluenesulfonyloxymethyl-5-(4-tert-butylbenzyl)thio-3(2H)-pyridazinone (1044696-16-3)

Guidance literature:

With pyridine; for 4h;

upstream raw materials:

2-tert-butyl-4-(tert-butyldimethylsilyloxy)methyl-5-(4-tert-butylbenzyl)mercapto-3-(2H)-pyridazinone

Downstream raw materials:

2-tert-butyl-4-p-toluenesulfonyloxymethyl-5-(4-tert-butylbenzyl)thio-3(2H)-pyridazinone

2-tert-butyl-4-(methanesulfonyloxy)methyl-5-(4-tert-butylbenzyl)mercapto-3-(2H)-pyridazinone

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