C₂₇H₂₆N₂O₆

Base Information

Chemical Name:C₂₇H₂₆N₂O₆
CAS No.:1275620-45-5
Molecular Formula:C₂₇H₂₆N₂O₆
Molecular Weight:474.513
Hs Code.:

C<sub>27</sub>H<sub>26</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₂₇H₂₆N₂O₆

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Chemical Property of C₂₇H₂₆N₂O₆

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Technology Process of C₂₇H₂₆N₂O₆

There total 12 articles about C₂₇H₂₆N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.3%

: 1275620-44-4
4-chloro-2-phenyl-benzofuro[3,2-b]pyridine

: 1275620-45-5
C₂₇H₂₆N₂O₆

Guidance literature:: (2S,4R)-4-hydroxy-1-[(2-methylpropan-2-yl)oxycarbonyl]pyrrolidine-2-carboxylic acid; With sodium t-butanolate; In dimethyl sulfoxide; at 0 - 20 ℃; for 1h;

4-chloro-2-phenyl-benzofuro[3,2-b]pyridine; In dimethyl sulfoxide; at 10 ℃; for 4h;

With hydrogenchloride; In water; dimethyl sulfoxide; pH=6 - 7;

Reference yield:

: 611-20-1
salicylonitrile

: 1275620-45-5
C₂₇H₂₆N₂O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / butanone / 0.5 h / 20 °C

1.2: 100 °C

2.1: ethanol; water / 5 - 10 °C

3.1: Warmed water bath

4.1: bromine / chloroform

5.1: potassium acetate / acetone

6.1: acetic acid; phosphoric acid / 5 h / Reflux

7.1: trichlorophosphate / 2 h / Reflux

8.1: sodium t-butanolate / dimethyl sulfoxide / 1 h / 0 - 20 °C

8.2: 4 h / 10 °C

8.3: pH 6 - 7

With phosphoric acid; bromine; potassium acetate; potassium carbonate; acetic acid; sodium t-butanolate; trichlorophosphate; In ethanol; chloroform; water; dimethyl sulfoxide; acetone; butanone;

Reference yield:

: 2-phenyl-1,4-dihydrobenzofuro[2,3-b]pyridin-4-one

: 1275620-45-5
C₂₇H₂₆N₂O₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate / 2 h / Reflux

2.1: sodium t-butanolate / dimethyl sulfoxide / 1 h / 0 - 20 °C

2.2: 4 h / 10 °C

2.3: pH 6 - 7

With sodium t-butanolate; trichlorophosphate; In dimethyl sulfoxide;