methyl 2-(benzyloxy)-1-((tert-butoxycarbonyl)amino)cyclopentanecarboxylate

Base Information

Chemical Name:methyl 2-(benzyloxy)-1-((tert-butoxycarbonyl)amino)cyclopentanecarboxylate
CAS No.:1453267-34-9
Molecular Formula:C₁₉H₂₇NO₅
Molecular Weight:349.427
Hs Code.:

Synonyms:methyl 2-(benzyloxy)-1-((tert-butoxycarbonyl)amino)cyclopentanecarboxylate

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Chemical Property of methyl 2-(benzyloxy)-1-((tert-butoxycarbonyl)amino)cyclopentanecarboxylate

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Technology Process of methyl 2-(benzyloxy)-1-((tert-butoxycarbonyl)amino)cyclopentanecarboxylate

There total 6 articles about methyl 2-(benzyloxy)-1-((tert-butoxycarbonyl)amino)cyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 1244671-74-6
2-(benzyloxy)-1-((tert-butoxycarbonyl)amino)cyclopentanecarboxylic acid

: 1453267-34-9
methyl 2-(benzyloxy)-1-((tert-butoxycarbonyl)amino)cyclopentanecarboxylate

Guidance literature:: In diethyl ether; at 0 ℃; for 0.5h;

Reference yield:

: 4065-92-3,86703-52-8
cyclopentane-1,2-diol

: 1453267-34-9
methyl 2-(benzyloxy)-1-((tert-butoxycarbonyl)amino)cyclopentanecarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C

1.2: 24 h / 20 °C

2.1: Jones reagent / acetone / 0 °C

3.1: ammonium chloride / water; ethanol / 15 h / 20 °C

3.2: 48 h / 100 °C

4.1: sodium hydroxide / 19 h / 100 °C / Sealed tube

4.2: 18 h / 20 °C

5.1: diethyl ether / 0.5 h / 0 °C

With Jones reagent; sodium hydride; ammonium chloride; sodium hydroxide; In tetrahydrofuran; diethyl ether; ethanol; water; acetone;

Reference yield:

: 142-29-0
cyclopentene

: 1453267-34-9
methyl 2-(benzyloxy)-1-((tert-butoxycarbonyl)amino)cyclopentanecarboxylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / toluene; acetone; water / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C

2.2: 24 h / 20 °C

3.1: Jones reagent / acetone / 0 °C

4.1: ammonium chloride / water; ethanol / 15 h / 20 °C

4.2: 48 h / 100 °C

5.1: sodium hydroxide / 19 h / 100 °C / Sealed tube

5.2: 18 h / 20 °C

6.1: diethyl ether / 0.5 h / 0 °C

With osmium(VIII) oxide; Jones reagent; sodium hydride; ammonium chloride; 4-methylmorpholine N-oxide; sodium hydroxide; In tetrahydrofuran; diethyl ether; ethanol; water; acetone; toluene;