4-hydroxy-3-methoxycinnamate vinyl ester

Base Information

• Chemical Name: 4-hydroxy-3-methoxycinnamate vinyl ester
• CAS No.: 938433-11-5
• Molecular Formula: C₁₂H₁₂O₄
• Molecular Weight: 220.225
• Mol file: 938433-11-5.mol

Synonyms:4-hydroxy-3-methoxycinnamate vinyl ester

Chemical Property of 4-hydroxy-3-methoxycinnamate vinyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-hydroxy-3-methoxycinnamate vinyl ester

There total 2 articles about 4-hydroxy-3-methoxycinnamate vinyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

vinyl acetate (108-05-4,9003-20-7) + 3-(4-hydroxy-3-methoxyphenyl)acrylic acid (1135-24-6,537-98-4) → 4-hydroxy-3-methoxycinnamate vinyl ester (938433-11-5)

Guidance literature:

With mercury(II) diacetate; toluene-4-sulfonic acid; In tetrahydrofuran; at 20 ℃; Molecular sieve;

DOI:10.1016/j.bmcl.2013.07.051

Reference yield:

→ 4-hydroxy-3-methoxycinnamate vinyl ester (938433-11-5)

Guidance literature:

With Mercurous acetate; In tetrahydrofuran; for 0.05h; Inert atmosphere; Sealed tube;

With sulfuric acid; In tetrahydrofuran; at 60 - 65 ℃; for 12h; Inert atmosphere; Sealed tube;

Reference yield: 69.0%

4-hydroxy-3-methoxycinnamate vinyl ester (938433-11-5) + methyl-alpha-D-glucopyranoside (97-30-3) → methyl 6-O-feruloyl-α-D-glucopyranoside

Guidance literature:

With Lipolase 100T; In acetonitrile; at 20 - 37 ℃; for 64h; regioselective reaction; Enzymatic reaction;

DOI:10.1016/j.bmcl.2013.07.051

upstream raw materials:

vinyl acetate

3-(4-hydroxy-3-methoxyphenyl)acrylic acid

Downstream raw materials:

acetaldehyde

3-(4-hydroxy-3-methoxyphenyl)acrylic acid

ferulic acid 3',3'-dimethylallyl ester