C₄₉H₄₆ClN₅O₁₁P^(1-)

Base Information

Chemical Name:C₄₉H₄₆ClN₅O₁₁P^(1-)
CAS No.:75933-83-4
Molecular Formula:C₄₉H₄₆ClN₅O₁₁P
Molecular Weight:947.358
Hs Code.:

C<sub>49</sub>H<sub>46</sub>ClN<sub>5</sub>O<sub>11</sub>P<sup>(1-)</sup>

Synonyms:C₄₉H₄₆ClN₅O₁₁P^(1-)

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Chemical Property of C₄₉H₄₆ClN₅O₁₁P^(1-)

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Technology Process of C₄₉H₄₆ClN₅O₁₁P^(1-)

There total 4 articles about C₄₉H₄₆ClN₅O₁₁P^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75933-80-1
5'-O-(dimethoxytrityl)-2'-O-(tetrahydropyranyl)-N⁶-benzoyladenosine-3'-(4-chlorophenyl 5-chloro-8-quinolyl-phosphate)

: 75933-83-4
C₄₉H₄₆ClN₅O₁₁P^(1-)

Guidance literature:: With N₁,N₁,N₃,N₃-tetrametylquanidium salt of 2-pyridinecarboxaldehyde oxim; In 1,4-dioxane; water; at 22 ℃; for 16h;
DOI:10.1021/jo00316a020

Reference yield:

: 77181-81-8
4-chlorophenyl 5-chloro-8-quinolyl phosphorotetrazolide

: 75933-83-4
C₄₉H₄₆ClN₅O₁₁P^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0.5 h / 20 °C

2: N¹,N¹,N³,N³-tetramethylguanidium salt of pyridine-2-carboaldoxime / dioxane; H₂O / 16 h / 22 °C

With N₁,N₁,N₃,N₃-tetrametylquanidium salt of 2-pyridinecarboxaldehyde oxim; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/jo00316a020

Reference yield:

: 77181-80-7
Phosphorochloridic acid 4-chloro-phenyl ester 5-chloro-quinolin-8-yl ester

: 75933-83-4
C₄₉H₄₆ClN₅O₁₁P^(1-)

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 0.33 h

2: tetrahydrofuran / 0.5 h / 20 °C

3: N¹,N¹,N³,N³-tetramethylguanidium salt of pyridine-2-carboaldoxime / dioxane; H₂O / 16 h / 22 °C

With N₁,N₁,N₃,N₃-tetrametylquanidium salt of 2-pyridinecarboxaldehyde oxim; triethylamine; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/jo00316a020